3-[2-(2-{4-[2-(4-Benzyloxy-phenyl)-2-oxo-acetyl]-phenoxy}-ethoxy)-ethoxy]-5-hydroxy-benzoic acid methyl ester

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Chemical Name:3-[2-(2-{4-[2-(4-Benzyloxy-phenyl)-2-oxo-acetyl]-phenoxy}-ethoxy)-ethoxy]-5-hydroxy-benzoic acid methyl ester
CAS No.:885058-84-4
Molecular Formula:C₃₃H₃₀O₉
Molecular Weight:570.596
Hs Code.:

Synonyms:3-[2-(2-{4-[2-(4-Benzyloxy-phenyl)-2-oxo-acetyl]-phenoxy}-ethoxy)-ethoxy]-5-hydroxy-benzoic acid methyl ester

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Chemical Property of 3-[2-(2-{4-[2-(4-Benzyloxy-phenyl)-2-oxo-acetyl]-phenoxy}-ethoxy)-ethoxy]-5-hydroxy-benzoic acid methyl ester

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Technology Process of 3-[2-(2-{4-[2-(4-Benzyloxy-phenyl)-2-oxo-acetyl]-phenoxy}-ethoxy)-ethoxy]-5-hydroxy-benzoic acid methyl ester

There total 6 articles about 3-[2-(2-{4-[2-(4-Benzyloxy-phenyl)-2-oxo-acetyl]-phenoxy}-ethoxy)-ethoxy]-5-hydroxy-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 885058-80-0
1-(4-benzyloxy-phenyl)-2-{4-[2-(2-iodo-ethoxy)-ethoxy]-phenyl}-ethane-1,2-dione

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 885058-84-4
3-[2-(2-{4-[2-(4-Benzyloxy-phenyl)-2-oxo-acetyl]-phenoxy}-ethoxy)-ethoxy]-5-hydroxy-benzoic acid methyl ester

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 16h;
DOI:10.1021/ol060025o

Reference yield:

: 885058-71-9
4-benzyloxy-4'-hydroxybenzil

: 885058-84-4
3-[2-(2-{4-[2-(4-Benzyloxy-phenyl)-2-oxo-acetyl]-phenoxy}-ethoxy)-ethoxy]-5-hydroxy-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / Cs₂CO₃ / dimethylformamide / 100 °C

2: iPr₂NEt / CH₂Cl₂; dimethylformamide / 2 h / 0 °C

3: NaI / acetone / Heating

4: 55 percent / Cs₂CO₃ / dimethylformamide / 16 h / 100 °C

With caesium carbonate; N-ethyl-N,N-diisopropylamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol060025o

Reference yield:

: 885058-78-6
1-(4-benzyloxy-phenyl)-2-{4-[2-(2-hydroxy-ethoxy)-ethoxy]-phenyl}-ethane-1,2-dione

: 885058-84-4
3-[2-(2-{4-[2-(4-Benzyloxy-phenyl)-2-oxo-acetyl]-phenoxy}-ethoxy)-ethoxy]-5-hydroxy-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: iPr₂NEt / CH₂Cl₂; dimethylformamide / 2 h / 0 °C

2: NaI / acetone / Heating

3: 55 percent / Cs₂CO₃ / dimethylformamide / 16 h / 100 °C

With caesium carbonate; N-ethyl-N,N-diisopropylamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol060025o