(-)-(αR,βS)-4,4',6'-trimethoxy-2'-O-methoxymethylchalcone epoxide

Base Information

• Chemical Name: (-)-(αR,βS)-4,4',6'-trimethoxy-2'-O-methoxymethylchalcone epoxide
• CAS No.: 130322-28-0
• Molecular Formula: C₂₀H₂₂O₇
• Molecular Weight: 374.39
• Mol file: 130322-28-0.mol

Synonyms:(-)-(αR,βS)-4,4',6'-trimethoxy-2'-O-methoxymethylchalcone epoxide

Chemical Property of (-)-(αR,βS)-4,4',6'-trimethoxy-2'-O-methoxymethylchalcone epoxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (-)-(αR,βS)-4,4',6'-trimethoxy-2'-O-methoxymethylchalcone epoxide

There total 3 articles about (-)-(αR,βS)-4,4',6'-trimethoxy-2'-O-methoxymethylchalcone epoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-2'-Methoxymethoxy-4,4',6'-trimethoxy-chalcon (35491-99-7) → (-)-(αR,βS)-4,4',6'-trimethoxy-2'-O-methoxymethylchalcone epoxide (130322-28-0) + (+)-(αS,βR)-4,4',6'-trimethoxy-2'-O-methoxymethylchalcone epoxide

Guidance literature:

With sodium hydroxide; poly-L-alanine; dihydrogen peroxide; In tetrachloromethane; water; Title compound not separated from byproducts; Ambient temperature;

DOI:10.1016/S0040-4020(97)00916-2

Reference yield:

trans-2'-Methoxymethoxy-4,4',6'-trimethoxy-chalcon (35491-99-7) → (-)-(αR,βS)-4,4',6'-trimethoxy-2'-O-methoxymethylchalcone epoxide (130322-28-0)

Guidance literature:

With immobilised poly-(L)-leucine; urea-hydrogen peroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; for 96h; Yield given; Ambient temperature;

DOI:10.1016/S0040-4020(99)00554-2

Reference yield:

→ (-)-(αR,βS)-4,4',6'-trimethoxy-2'-O-methoxymethylchalcone epoxide (130322-28-0)

Guidance literature:

upstream raw materials:

trans-2'-Methoxymethoxy-4,4',6'-trimethoxy-chalcon

Downstream raw materials:

2-hydroxy-3-(4-methoxyphenyl)-3-(3,5-dimethoxyphenoxy)-4',6'-dimethoxy-2'-methoxymethoxypropiophenone

1-(4,6-dimethoxy-2-methoxymethoxyphenyl)-3-(4-methoxyphenyl)-3-(2-hydroxy-4,6-dimethoxyphenyl)propane-1,2-dione

2-hydroxy-3-(4-methoxyphenyl)-3-(2-hydroxy-4,6-dimethoxyphenyl)-4',6'-dimethoxy-2'-methoxymethoxypropiophenone

1-hydroxy-1-(4,6-dimethoxy-2-methoxymethoxyphenyl)-3-(4-methoxyphenyl)-3-(2-hydroxy-4,6-dimethoxyphenyl)propan-2-one