Technology Process of C34H37FN4O8S
There total 10 articles about C34H37FN4O8S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
for 3h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: lithium hydroxide; water / tetrahydrofuran / 1.5 h / 0 °C
1.2: pH 4
2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0.5 h / 0 °C
2.2: 17 h / 20 °C
3.1: titanium(IV) isopropylate; titanium tetrachloride / dichloromethane / 0.5 h / 0 °C
3.2: 0.83 h / -30 - 0 °C
4.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 1 h / 90 °C
4.2: 2 h / 45 °C
5.1: formic acid / 1.5 h
6.1: 4-methyl-morpholine / dichloromethane / 20 °C
6.3: 2 h
7.1: 4-methyl-morpholine / dichloromethane / 20 °C
7.2: 2 h
8.1: trifluoroacetic acid / dichloromethane / 3 h
With
4-methyl-morpholine; titanium(IV) isopropylate; dmap; lithium hydroxide; formic acid; water; titanium tetrachloride; N,O-bis-(trimethylsilyl)-acetamide; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: formic acid / 1.5 h
2.1: 4-methyl-morpholine / dichloromethane / 20 °C
2.3: 2 h
3.1: 4-methyl-morpholine / dichloromethane / 20 °C
3.2: 2 h
4.1: trifluoroacetic acid / dichloromethane / 3 h
With
4-methyl-morpholine; formic acid; trifluoroacetic acid;
In
dichloromethane;
