α-deuterio-cis-5-methyl-2-cyclohexenyl mesitoate

Base Information

• Chemical Name: α-deuterio-cis-5-methyl-2-cyclohexenyl mesitoate
• CAS No.: 102853-25-8
• Molecular Formula: C₁₇H₂₂O₂
• Molecular Weight: 259.353
• Mol file: 102853-25-8.mol

Synonyms:α-deuterio-cis-5-methyl-2-cyclohexenyl mesitoate

Chemical Property of α-deuterio-cis-5-methyl-2-cyclohexenyl mesitoate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of α-deuterio-cis-5-methyl-2-cyclohexenyl mesitoate

There total 1 articles about α-deuterio-cis-5-methyl-2-cyclohexenyl mesitoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-1-deuterio-5-methyl-2-cyclohexen-1-ol (73964-44-0) + mesitylene-2-carboxylic acid chloride (938-18-1) → α-deuterio-cis-5-methyl-2-cyclohexenyl mesitoate (102853-25-8)

Guidance literature:

In pyridine; Ambient temperature;

DOI:10.1021/jo00365a006

Reference yield: 63.0%

n-butyl magnesium bromide (693-03-8) + α-deuterio-cis-5-methyl-2-cyclohexenyl mesitoate (102853-25-8) → C11H19(2)H

Guidance literature:

With CuCN; In diethyl ether; for 6.5h; Ambient temperature;

DOI:10.1021/jo00365a006

Reference yield:

n-butyl magnesium bromide (693-03-8) + α-deuterio-cis-5-methyl-2-cyclohexenyl mesitoate (102853-25-8) → C11H19(2)H + C11H19(2)H

Guidance literature:

With copper(l) chloride; In diethyl ether; for 6.5h; Ambient temperature;

DOI:10.1021/jo00365a006

upstream raw materials:

cis-1-deuterio-5-methyl-2-cyclohexen-1-ol

mesitylene-2-carboxylic acid chloride