N²-[(4-tert-butyl)benzoyl]-N⁴-tert-butoxycarbonyl-N¹-(4-methoxybenzoyl)-1,2,4-benzenetriamine

Base Information

• Chemical Name: N²-[(4-tert-butyl)benzoyl]-N⁴-tert-butoxycarbonyl-N¹-(4-methoxybenzoyl)-1,2,4-benzenetriamine
• CAS No.: 263841-64-1
• Molecular Formula: C₃₀H₃₅N₃O₅
• Molecular Weight: 517.625

Synonyms:N²-[(4-tert-butyl)benzoyl]-N⁴-tert-butoxycarbonyl-N¹-(4-methoxybenzoyl)-1,2,4-benzenetriamine

Chemical Property of N²-[(4-tert-butyl)benzoyl]-N⁴-tert-butoxycarbonyl-N¹-(4-methoxybenzoyl)-1,2,4-benzenetriamine

Chemical Property:

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Technology Process of N²-[(4-tert-butyl)benzoyl]-N⁴-tert-butoxycarbonyl-N¹-(4-methoxybenzoyl)-1,2,4-benzenetriamine

There total 2 articles about N²-[(4-tert-butyl)benzoyl]-N⁴-tert-butoxycarbonyl-N¹-(4-methoxybenzoyl)-1,2,4-benzenetriamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N1-[(4-methoxy)benzoyl]-N4-tert-butoxycarbonyl-2-nitro-1,4-benzenediamine → N2-[(4-tert-butyl)benzoyl]-N4-tert-butoxycarbonyl-N1-(4-methoxybenzoyl)-1,2,4-benzenetriamine (263841-64-1)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd/C / tetrahydrofuran

2: pyridine / CH₂Cl₂

With pyridine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; 1: Reduction / 2: Acylation;

DOI:10.1021/jm990326m

Reference yield:

N1-[(4-methoxy)benzoyl]-N4-tert-butoxycarbonyl-1,2,4-benzenetriamine (263841-63-0) + p-tert-butyl benzoyl chloride (1710-98-1) → N2-[(4-tert-butyl)benzoyl]-N4-tert-butoxycarbonyl-N1-(4-methoxybenzoyl)-1,2,4-benzenetriamine (263841-64-1)

Guidance literature:

With pyridine; In dichloromethane;

DOI:10.1021/jm990326m

Reference yield:

N2-[(4-tert-butyl)benzoyl]-N4-tert-butoxycarbonyl-N1-(4-methoxybenzoyl)-1,2,4-benzenetriamine (263841-64-1) → N2-(4-tert-butylbenzoyl)-N1-(4-methoxybenzoyl)-1,2,4-benzenetriamine (263841-84-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1021/jm990326m

upstream raw materials:

N¹-[(4-methoxy)benzoyl]-N⁴-tert-butoxycarbonyl-1,2,4-benzenetriamine

p-tert-butyl benzoyl chloride

Downstream raw materials:

N²-(4-tert-butylbenzoyl)-N¹-(4-methoxybenzoyl)-1,2,4-benzenetriamine

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