benzyl 3,6-di-O-benzyl-2-deoxy-2-N-glycolyl-5-O-methyl-α-D-mannofuranoside

Base Information

Chemical Name:benzyl 3,6-di-O-benzyl-2-deoxy-2-N-glycolyl-5-O-methyl-α-D-mannofuranoside
CAS No.:1332835-25-2
Molecular Formula:C₃₀H₃₅NO₇
Molecular Weight:521.61
Hs Code.:

Synonyms:benzyl 3,6-di-O-benzyl-2-deoxy-2-N-glycolyl-5-O-methyl-α-D-mannofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3,6-di-O-benzyl-2-deoxy-2-N-glycolyl-5-O-methyl-α-D-mannofuranoside

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Technology Process of benzyl 3,6-di-O-benzyl-2-deoxy-2-N-glycolyl-5-O-methyl-α-D-mannofuranoside

There total 11 articles about benzyl 3,6-di-O-benzyl-2-deoxy-2-N-glycolyl-5-O-methyl-α-D-mannofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 19374-87-9
(2,5-dioxopyrrolidin-1-yl) 2-hydroxyacetate

: 119870-39-2
benzyl 3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranosamine

: 1332835-25-2
benzyl 3,6-di-O-benzyl-2-deoxy-2-N-glycolyl-5-O-methyl-α-D-mannofuranoside

Guidance literature:: In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.04.083

Reference yield:

: 1332835-24-1
benzyl 2-azido-3-O-benzyl-2-deoxy-α-D-manofuranoside

: 1332835-25-2
benzyl 3,6-di-O-benzyl-2-deoxy-2-N-glycolyl-5-O-methyl-α-D-mannofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: di(n-butyl)tin oxide / toluene / 2 h / Reflux

1.2: 24 h / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h

2.2: 20 °C

3.1: 1.3-propanedithiol; triethylamine / pyridine; water / 24 h / 50 °C

4.1: N,N-dimethyl-formamide

With 1.3-propanedithiol; sodium hydride; di(n-butyl)tin oxide; triethylamine; In pyridine; water; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1016/j.bmcl.2011.04.083

Reference yield:

: C₂₂H₂₁F₃O₉S

: 1332835-25-2
benzyl 3,6-di-O-benzyl-2-deoxy-2-N-glycolyl-5-O-methyl-α-D-mannofuranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium azide / N,N-dimethyl-formamide / 0 - 20 °C

2.1: sodium methylate / methanol / 20 °C

3.1: di(n-butyl)tin oxide / toluene / 2 h / Reflux

3.2: 24 h / Inert atmosphere; Reflux

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h

4.2: 20 °C

5.1: 1.3-propanedithiol; triethylamine / pyridine; water / 24 h / 50 °C

6.1: N,N-dimethyl-formamide

With 1.3-propanedithiol; sodium azide; sodium methylate; sodium hydride; di(n-butyl)tin oxide; triethylamine; In pyridine; methanol; water; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1016/j.bmcl.2011.04.083