N^α-benzyloxycarbonyl-N^ε-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester

Base Information

Chemical Name:N^α-benzyloxycarbonyl-N^ε-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester
CAS No.:648910-27-4
Molecular Formula:C₂₁H₃₀N₂O₆
Molecular Weight:406.479
Hs Code.:

N<sup>α</sup>-benzyloxycarbonyl-N<sup>ε</sup>-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester

Synonyms:N^α-benzyloxycarbonyl-N^ε-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester

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Chemical Property of N^α-benzyloxycarbonyl-N^ε-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester

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Technology Process of N^α-benzyloxycarbonyl-N^ε-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester

There total 5 articles about N^α-benzyloxycarbonyl-N^ε-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 706810-26-6
N^ε-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester

: 648910-27-4
N^α-benzyloxycarbonyl-N^ε-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2004.03.028

Reference yield:

: 13515-95-2,15445-34-8,26348-70-9,34015-48-0,67396-08-1,130336-19-5
lysine methyl ester dihydrochloride

: 648910-27-4
N^α-benzyloxycarbonyl-N^ε-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 1.5 h / 20 °C

2: 69 percent / triethylamine / CH₂Cl₂ / 2 h / 20 °C

With dmap; triethylamine; In dichloromethane;
DOI:10.1016/j.tet.2004.03.028

Reference yield:

: 556-82-1
3-methyl-2-buten-1-ol

: 648910-27-4
N^α-benzyloxycarbonyl-N^ε-(3-methyl-2-butenyl)oxycarbonyl-L-lysine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / pyridine / CH₂Cl₂ / 16 h / 20 °C

2: 81 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 1.5 h / 20 °C

3: 69 percent / triethylamine / CH₂Cl₂ / 2 h / 20 °C

With pyridine; dmap; triethylamine; In dichloromethane;
DOI:10.1016/j.tet.2004.03.028