C₃₂H₄₂N₂O₄Si

Base Information

Chemical Name:C₃₂H₄₂N₂O₄Si
CAS No.:1269788-69-3
Molecular Formula:C₃₂H₄₂N₂O₄Si
Molecular Weight:546.782
Hs Code.:

C<sub>32</sub>H<sub>42</sub>N<sub>2</sub>O<sub>4</sub>Si

Synonyms:C₃₂H₄₂N₂O₄Si

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Chemical Property of C₃₂H₄₂N₂O₄Si

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Technology Process of C₃₂H₄₂N₂O₄Si

There total 1 articles about C₃₂H₄₂N₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1269788-58-0
C₃₂H₄₄N₂O₅Si

: 1269788-69-3
C₃₂H₄₂N₂O₄Si

Guidance literature:: C₃₂H₄₄N₂O₅Si; With Trimethyl orthoacetate; pyridinium p-toluenesulfonate; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

With chloro-trimethyl-silane; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

With potassium carbonate; In methanol; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.12.066

Reference yield:

: 1269788-69-3
C₃₂H₄₂N₂O₄Si

: 56-54-2,130-95-0,572-59-8,572-60-1,42151-59-7,47342-58-5,72402-50-7,72402-51-8,72402-52-9,72402-53-0,101143-86-6,101143-87-7,101143-88-8,146925-10-2
quinindine

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / hexane; toluene / 0.33 h / -78 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide / 4 h / Reflux; Inert atmosphere

3.1: dmap; triethylamine / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

4.1: hydrogenchloride; methanol / 5 h / 20 °C / Inert atmosphere

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere

5.2: -78 - 0 °C / Inert atmosphere

6.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

6.2: 0.5 h / 0 °C

7.1: methanol; potassium carbonate / 1.5 h / 20 °C / Inert atmosphere

With hydrogenchloride; methanol; dmap; oxalyl dichloride; potassium tert-butylate; diisobutylaluminium hydride; potassium carbonate; dimethyl sulfoxide; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; hexane; dichloromethane; toluene; 5.1: Swern oxidation / 5.2: Swern oxidation / 6.1: Wittig reaction / 6.2: Wittig reaction;
DOI:10.1016/j.tetlet.2010.12.066

Reference yield:

: 1269788-69-3
C₃₂H₄₂N₂O₄Si

: 56652-53-0
quinidine acetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / hexane; toluene / 0.33 h / -78 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide / 4 h / Reflux; Inert atmosphere

3.1: dmap; triethylamine / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

4.1: hydrogenchloride; methanol / 5 h / 20 °C / Inert atmosphere

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere

5.2: -78 - 0 °C / Inert atmosphere

6.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

6.2: 0.5 h / 0 °C

With hydrogenchloride; methanol; dmap; oxalyl dichloride; potassium tert-butylate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; hexane; dichloromethane; toluene; 5.1: Swern oxidation / 5.2: Swern oxidation / 6.1: Wittig reaction / 6.2: Wittig reaction;
DOI:10.1016/j.tetlet.2010.12.066