octyl 6-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-2,3,5-tri-O-benzyl-β-D-galactofuranoside

Base Information

Chemical Name:octyl 6-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-2,3,5-tri-O-benzyl-β-D-galactofuranoside
CAS No.:189315-17-1
Molecular Formula:C₄₉H₆₄O₁₅
Molecular Weight:893.038
Hs Code.:

Synonyms:octyl 6-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-2,3,5-tri-O-benzyl-β-D-galactofuranoside

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Chemical Property of octyl 6-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-2,3,5-tri-O-benzyl-β-D-galactofuranoside

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Technology Process of octyl 6-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-2,3,5-tri-O-benzyl-β-D-galactofuranoside

There total 10 articles about octyl 6-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-2,3,5-tri-O-benzyl-β-D-galactofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 212781-54-9
pent-4-enyl 2,3,5,6-tetra-O-acetyl-α,β-D-galactofuranoside

: 189315-16-0
octyl 2,3,5-tri-O-benzyl-β-D-galactofuranoside

: 189315-17-1
octyl 6-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-2,3,5-tri-O-benzyl-β-D-galactofuranoside

Guidance literature:: With N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate; In dichloromethane; at 20 ℃;
DOI:10.1016/S0008-6215(96)00268-6

Reference yield:

: 189315-16-0
octyl 2,3,5-tri-O-benzyl-β-D-galactofuranoside

: 514847-70-2
pyrimidin-2-yl 2,3,5,6-tetra-O-acetyl-1-thio-β-D-galactofuranoside

: 189315-17-1
octyl 6-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-2,3,5-tri-O-benzyl-β-D-galactofuranoside

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃;
DOI:10.1016/j.carres.2006.10.001

Reference yield:

: 166021-57-4
n-octyl β-D-galactofuranoside

: 189315-17-1
octyl 6-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-2,3,5-tri-O-benzyl-β-D-galactofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / CH₂Cl₂ / 24 h / Heating

2: 99 percent / NaH / 20 °C

3: 78 percent / acetic acid / H₂O / 20 °C

4: Cu(OTf)2 / CH₂Cl₂ / 20 °C

With copper(II) bis(trifluoromethanesulfonate); sodium hydride; acetic acid; In dichloromethane; water;
DOI:10.1016/j.carres.2006.10.001