C₃₉H₆₀O₄Si₂

Base Information

Chemical Name:C₃₉H₆₀O₄Si₂
CAS No.:1404304-74-0
Molecular Formula:C₃₉H₆₀O₄Si₂
Molecular Weight:649.074
Hs Code.:

C<sub>39</sub>H<sub>60</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₉H₆₀O₄Si₂

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Chemical Property of C₃₉H₆₀O₄Si₂

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Technology Process of C₃₉H₆₀O₄Si₂

There total 11 articles about C₃₉H₆₀O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1404304-73-9
C₂₈H₃₈O₂Si

: 214483-35-9
tert-Butyl-dimethyl-((S)-(R)-1-oxiranyl-allyloxy)-silane

: 1404304-74-0
C₃₉H₆₀O₄Si₂

Guidance literature:: C₂₈H₃₈O₂Si; With n-butyllithium; In tetrahydrofuran; hexane; at -40 ℃; for 0.5h; Inert atmosphere;

tert-Butyl-dimethyl-((S)-(R)-1-oxiranyl-allyloxy)-silane; With boron trifluoride diethyl etherate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.25h; Inert atmosphere;
DOI:10.1021/ol302409g

Reference yield:

: 102517-37-3
(2R,3R)-1,2-epoxy-3-heptanol

: 1404304-74-0
C₃₉H₆₀O₄Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1H-imidazole / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

2.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 1 h / -78 - 20 °C / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 6 h / 40 °C / Inert atmosphere

4.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl) / tetrahydrofuran / 50 °C / Inert atmosphere

5.1: triethylamine / methanol / 0.75 h / 20 °C / Inert atmosphere

6.1: triphenylphosphine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 0.83 h / -78 - -30 °C / Inert atmosphere

8.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -40 °C / Inert atmosphere

8.2: 1.25 h / -78 - 20 °C / Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; copper(l) iodide; n-butyllithium; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ol302409g

Reference yield:

: 1404304-64-8
C₂₃H₃₂O₂Si

: 1404304-74-0
C₃₉H₆₀O₄Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 1 h / -78 - 20 °C / Inert atmosphere

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 6 h / 40 °C / Inert atmosphere

3.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl) / tetrahydrofuran / 50 °C / Inert atmosphere

4.1: triethylamine / methanol / 0.75 h / 20 °C / Inert atmosphere

5.1: triphenylphosphine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.83 h / -78 - -30 °C / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -40 °C / Inert atmosphere

7.2: 1.25 h / -78 - 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; copper(l) iodide; n-butyllithium; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ol302409g