methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside
CAS No.:1426575-71-4
Molecular Formula:C₈₂H₈₄O₁₇
Molecular Weight:1341.56
Hs Code.:

methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside

Synonyms:methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside

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Chemical Property of methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside

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Technology Process of methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside

There total 2 articles about methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1319712-48-5
methyl 3-O-benzoyl-2,6-di-O-benzyl-α-D-glucopyranoside

: C₅₇H₅₈Cl₃NO₁₁

: 1426575-71-4
methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -20 ℃; Inert atmosphere;
DOI:10.1016/j.carres.2012.12.015

Reference yield:

: 1319712-48-5
methyl 3-O-benzoyl-2,6-di-O-benzyl-α-D-glucopyranoside

: 1426575-72-5
C₆₀H₆₀O₁₀S

: 1426575-71-4
methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside

: methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In diethyl ether; dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1016/j.carres.2012.12.015

Reference yield: 71.0%

: 1426575-71-4
methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-benzoyl-α-D-glucopyranoside

: 1426575-74-7
methyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-α-D-glucopyranoside

Guidance literature:: With cesiumhydroxide monohydrate; sodium; In methanol; for 16h; Reagent/catalyst; Solvent;
DOI:10.1016/j.carres.2012.12.015