methyl (Sp)-2-(diphenylphosphino)ferrocenecarboxylate

Base Information

• Chemical Name: methyl (Sp)-2-(diphenylphosphino)ferrocenecarboxylate
• CAS No.: 1083100-07-5
• Molecular Formula: C₂₄H₂₁FeO₂P
• Molecular Weight: 428.25

Synonyms:methyl (Sp)-2-(diphenylphosphino)ferrocenecarboxylate

Chemical Property of methyl (Sp)-2-(diphenylphosphino)ferrocenecarboxylate

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Technology Process of methyl (Sp)-2-(diphenylphosphino)ferrocenecarboxylate

There total 1 articles about methyl (Sp)-2-(diphenylphosphino)ferrocenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(S,Sp)-2-acetamido-3-methylbutyl 2-(diphenylphosphino)ferrocenecarboxylate → (Sp)-2-(diphenylphosphino)ferrocenecarboxylic acid (297176-74-0,847675-62-1,677722-99-5) + methyl (Sp)-2-(diphenylphosphino)ferrocenecarboxylate (1083100-07-5)

Guidance literature:

With aq. NaOH; In tetrahydrofuran; methanol; all manipulations under Ar; Fe compd. dissolved in mixt. of THF and MeOH, aq. NaOH soln. added, stirred at 50°C overnight; solvent removed, 3 M HCl added, extd. with CH2Cl2, washed with water, dried with MgSO4, evapd., chromy. (silica gel, CH2Cl2-MeOH (20:1)), evapd.dried in vac. (1 Torr, 60°C, 1 h), elem. anal.; Me-compd. identi fied by NMR;

DOI:10.1039/b109495p

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