1-<<4(S),5-bis(benzyloxy)-1-(diethylphosphonyl)-3(R)-pentoxy>methyl>thymine

Base Information

Chemical Name:1-<<4(S),5-bis(benzyloxy)-1-(diethylphosphonyl)-3(R)-pentoxy>methyl>thymine
CAS No.:174358-96-4
Molecular Formula:C₂₉H₃₉N₂O₈P
Molecular Weight:574.611
Hs Code.:

Synonyms:1-<<4(S),5-bis(benzyloxy)-1-(diethylphosphonyl)-3(R)-pentoxy>methyl>thymine

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Chemical Property of 1-<<4(S),5-bis(benzyloxy)-1-(diethylphosphonyl)-3(R)-pentoxy>methyl>thymine

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Technology Process of 1-<<4(S),5-bis(benzyloxy)-1-(diethylphosphonyl)-3(R)-pentoxy>methyl>thymine

There total 3 articles about 1-<<4(S),5-bis(benzyloxy)-1-(diethylphosphonyl)-3(R)-pentoxy>methyl>thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: ((3R,4S)-4,5-Bis-benzyloxy-3-chloromethoxy-pentyl)-phosphonic acid diethyl ester

: 7288-28-0
2,4-bis(trimethylsiloxy)-5-methylpyrimidine

: 174358-96-4
1-<<4(S),5-bis(benzyloxy)-1-(diethylphosphonyl)-3(R)-pentoxy>methyl>thymine

Guidance literature:: With tetraethylammonium iodide; In dichloromethane; for 12h; Heating;
DOI:10.1021/jo951701v

Reference yield:

: 65-71-4,28806-14-6,691841-57-3
thymin

: 174358-96-4
1-<<4(S),5-bis(benzyloxy)-1-(diethylphosphonyl)-3(R)-pentoxy>methyl>thymine

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium sulfate / Heating

2: 63 percent / tetraethylammonium iodide / CH₂Cl₂ / 12 h / Heating

With ammonium sulfate; tetraethylammonium iodide; In dichloromethane;
DOI:10.1021/jo951701v

Reference yield:

: ((3R,4S)-4,5-Bis-benzyloxy-3-hydroxy-pentyl)-phosphonic acid diethyl ester

: 174358-96-4
1-<<4(S),5-bis(benzyloxy)-1-(diethylphosphonyl)-3(R)-pentoxy>methyl>thymine

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / ethanol; CH₂Cl₂ / 5 h / 0 °C

2: 63 percent / tetraethylammonium iodide / CH₂Cl₂ / 12 h / Heating

With hydrogenchloride; tetraethylammonium iodide; In ethanol; dichloromethane;
DOI:10.1021/jo951701v