3-amino-2-methyl-9-phenyl-7-(2-thienyl)pyrido[3',2':4,5]-thieno[3,2-d]pyrimidine-4(3H)-one

Base Information

Chemical Name:3-amino-2-methyl-9-phenyl-7-(2-thienyl)pyrido[3',2':4,5]-thieno[3,2-d]pyrimidine-4(3H)-one
CAS No.:723745-77-5
Molecular Formula:C₂₀H₁₄N₄OS₂
Molecular Weight:390.489
Hs Code.:

Synonyms:3-amino-2-methyl-9-phenyl-7-(2-thienyl)pyrido[3',2':4,5]-thieno[3,2-d]pyrimidine-4(3H)-one

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Chemical Property of 3-amino-2-methyl-9-phenyl-7-(2-thienyl)pyrido[3',2':4,5]-thieno[3,2-d]pyrimidine-4(3H)-one

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Technology Process of 3-amino-2-methyl-9-phenyl-7-(2-thienyl)pyrido[3',2':4,5]-thieno[3,2-d]pyrimidine-4(3H)-one

There total 6 articles about 3-amino-2-methyl-9-phenyl-7-(2-thienyl)pyrido[3',2':4,5]-thieno[3,2-d]pyrimidine-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 443904-61-8
2-methyl-9-phenyl-7-(2-thienyl)pyrido[3',2':4,5]-thieno[3,2-d]oxazine-4-one

: 723745-77-5
3-amino-2-methyl-9-phenyl-7-(2-thienyl)pyrido[3',2':4,5]-thieno[3,2-d]pyrimidine-4(3H)-one

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Heating;
DOI:10.1080/10426500490467147

Reference yield:

: 3988-77-0,39078-33-6,69656-36-6
3-phenyl-1-thiophen-2-yl-propenone

: 723745-77-5
3-amino-2-methyl-9-phenyl-7-(2-thienyl)pyrido[3',2':4,5]-thieno[3,2-d]pyrimidine-4(3H)-one

Guidance literature:: Multi-step reaction with 6 steps

1: 43 percent / piperidine / ethanol / 4 h / Heating

2: 95 percent / sodium acetate trihydrate / ethanol / 2 h / Heating

3: 90 percent / NaOEt / ethanol / 0.08 h / Heating

4: 86 percent / NaOH / ethanol / 4 h / Heating

5: 84 percent / 4 h / Heating

6: 86 percent / N₂H₄*H₂O / ethanol / 2 h / Heating

With piperidine; sodium hydroxide; sodium ethanolate; sodium acetate; hydrazine hydrate; In ethanol;
DOI:10.1080/10426500490467147

Reference yield:

: 82127-11-5
4-phenyl-6-(thiophen-2-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile

: 723745-77-5
3-amino-2-methyl-9-phenyl-7-(2-thienyl)pyrido[3',2':4,5]-thieno[3,2-d]pyrimidine-4(3H)-one

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / sodium acetate trihydrate / ethanol / 2 h / Heating

2: 90 percent / NaOEt / ethanol / 0.08 h / Heating

3: 86 percent / NaOH / ethanol / 4 h / Heating

4: 84 percent / 4 h / Heating

5: 86 percent / N₂H₄*H₂O / ethanol / 2 h / Heating

With sodium hydroxide; sodium ethanolate; sodium acetate; hydrazine hydrate; In ethanol;
DOI:10.1080/10426500490467147