N-(6-formyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide

Base Information

Chemical Name:N-(6-formyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide
CAS No.:784202-87-5
Molecular Formula:C₃₀H₂₈N₂O₄S
Molecular Weight:512.629
Hs Code.:

<i>N</i>-(6-formyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide

Synonyms:N-(6-formyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide

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Chemical Property of N-(6-formyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide

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Technology Process of N-(6-formyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide

There total 8 articles about N-(6-formyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(6-hydroxymethyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide

: 784202-87-5
N-(6-formyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide

Guidance literature:: With manganese(IV) oxide; In dichloromethane; acetone; at 20 ℃; for 16h;
DOI:10.1021/jm061224g

Reference yield:

: 784205-23-8
(RS)-(5-amino-5,6,7,8-tetrahydronaphthalen-2-yl)methanol

: 784202-87-5
N-(6-formyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: HOBt; silica-supported carbodiimide / tetrahydrofuran; dimethylformamide / 36 h / 20 - 35 °C

2: MnO₂ / acetone; CH₂Cl₂ / 16 h / 20 °C

With manganese(IV) oxide; silica-supported carbodiimide; benzotriazol-1-ol; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm061224g

Reference yield:

: 361369-86-0
5-azido-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid methyl ester

: 784202-87-5
N-(6-formyl-1,2,3,4-tetrahydro-naphthalen-1-yl)-3-(naphthalene-2-sulfonylamino)-3-phenyl-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / tetrahydrofuran / -15 - 20 °C

2: HOBt; silica-supported carbodiimide / tetrahydrofuran; dimethylformamide / 36 h / 20 - 35 °C

3: MnO₂ / acetone; CH₂Cl₂ / 16 h / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; silica-supported carbodiimide; benzotriazol-1-ol; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm061224g