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Technology Process of S-ethyl 2-cyano-2-N.N'-di(tert-butoxycarbonyl)hydrazino-3-(4-methoxyphenyl)propanethioate

S-ethyl 2-cyano-2-N.N'-di(tert-butoxycarbonyl)hydrazino-3-(4-methoxyphenyl)propanethioate

Base Information
  • Chemical Name:S-ethyl 2-cyano-2-N.N'-di(tert-butoxycarbonyl)hydrazino-3-(4-methoxyphenyl)propanethioate
  • CAS No.:1217897-85-2
  • Molecular Formula:C23H33N3O6S
  • Molecular Weight:479.598
  • Hs Code.:
S-ethyl 2-cyano-2-N<sub>.</sub>N'-di(tert-butoxycarbonyl)hydrazino-3-(4-methoxyphenyl)propanethioate

Synonyms:S-ethyl 2-cyano-2-N.N'-di(tert-butoxycarbonyl)hydrazino-3-(4-methoxyphenyl)propanethioate

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Chemical Property of S-ethyl 2-cyano-2-N.N'-di(tert-butoxycarbonyl)hydrazino-3-(4-methoxyphenyl)propanethioate
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Technology Process of S-ethyl 2-cyano-2-N.N'-di(tert-butoxycarbonyl)hydrazino-3-(4-methoxyphenyl)propanethioate

There total 1 articles about S-ethyl 2-cyano-2-N.N'-di(tert-butoxycarbonyl)hydrazino-3-(4-methoxyphenyl)propanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

di-tert-butyl-diazodicarboxylate
870-50-8

di-tert-butyl-diazodicarboxylate

S-ethyl 2-cyano-3-(4-methoxyphenyl)propanethioate
1217897-87-4

S-ethyl 2-cyano-3-(4-methoxyphenyl)propanethioate

S-ethyl 2-cyano-2-N<sub>.</sub>N'-di(tert-butoxycarbonyl)hydrazino-3-(4-methoxyphenyl)propanethioate
1217897-85-2

S-ethyl 2-cyano-2-N.N'-di(tert-butoxycarbonyl)hydrazino-3-(4-methoxyphenyl)propanethioate

Guidance literature:
S-ethyl 2-cyano-3-(4-methoxyphenyl)propanethioate; With 2,6-bis-(3',5'-di-tert-butyl-biphenyl-4-yl)-3,5-dihydro-4-aza-cyclohepta[2,1-a;3,4-a']dinaphthalene-4-carboxamidine; In 1,2-dimethoxyethane; diethyl ether; at 20 ℃; for 0.25h; Inert atmosphere;
di-tert-butyl-diazodicarboxylate; In 1,2-dimethoxyethane; diethyl ether; at -80 ℃; for 1h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.200900594
upstream raw materials:

di-tert-butyl-diazodicarboxylate

S-ethyl 2-cyano-3-(4-methoxyphenyl)propanethioate

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