methyl (S)-2-[(S)-2-amino-6-azidohexanamido]-3-phenylpropanoate hydrochloride

Base Information

Chemical Name:methyl (S)-2-[(S)-2-amino-6-azidohexanamido]-3-phenylpropanoate hydrochloride
CAS No.:1414357-76-8
Molecular Formula:C₁₆H₂₃N₅O₃*ClH
Molecular Weight:369.851
Hs Code.:

Synonyms:methyl (S)-2-[(S)-2-amino-6-azidohexanamido]-3-phenylpropanoate hydrochloride

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Chemical Property of methyl (S)-2-[(S)-2-amino-6-azidohexanamido]-3-phenylpropanoate hydrochloride

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Technology Process of methyl (S)-2-[(S)-2-amino-6-azidohexanamido]-3-phenylpropanoate hydrochloride

There total 3 articles about methyl (S)-2-[(S)-2-amino-6-azidohexanamido]-3-phenylpropanoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1414357-73-5
methyl (S)-2-{(S)-6-azido-2-[(tert-butoxycarbonyl)amino]hexanamido}-3-phenylpropanoate

: 1414357-76-8
methyl (S)-2-[(S)-2-amino-6-azidohexanamido]-3-phenylpropanoate hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 2h;
DOI:10.1055/s-0032-1316702

Reference yield:

: 13734-28-6
Boc-Lys-OH

: 1414357-76-8
methyl (S)-2-[(S)-2-amino-6-azidohexanamido]-3-phenylpropanoate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; benzotriazol-1-yl-sulfonyl azide / water; acetonitrile / 6 h / 20 °C

2: N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; 1,2,3-Benzotriazole / acetonitrile / 0 - 20 °C

3: hydrogenchloride / methanol / 2 h / 20 °C

With hydrogenchloride; 1,2,3-Benzotriazole; benzotriazol-1-yl-sulfonyl azide; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In methanol; water; acetonitrile;
DOI:10.1055/s-0032-1316702

Reference yield:

: 846549-33-5
dicyclohexylammonium N-tert-butyloxycarbonyl-2-amino-6-azidohexanoate

: 1414357-76-8
methyl (S)-2-[(S)-2-amino-6-azidohexanamido]-3-phenylpropanoate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; 1,2,3-Benzotriazole / acetonitrile / 0 - 20 °C

2: hydrogenchloride / methanol / 2 h / 20 °C

With hydrogenchloride; 1,2,3-Benzotriazole; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In methanol; acetonitrile;
DOI:10.1055/s-0032-1316702