bis[ethyl(μ-4,6-di-tert-butyl-2-(N-phenylpiperazinyl-N'-methyl)phenoxo)zinc]

Base Information

Chemical Name:bis[ethyl(μ-4,6-di-tert-butyl-2-(N-phenylpiperazinyl-N'-methyl)phenoxo)zinc]
CAS No.:874750-74-0
Molecular Formula:C₅₄H₈₀N₄O₂Zn₂
Molecular Weight:948.035
Hs Code.:

Synonyms:bis[ethyl(μ-4,6-di-tert-butyl-2-(N-phenylpiperazinyl-N'-methyl)phenoxo)zinc]

Suppliers and Price of bis[ethyl(μ-4,6-di-tert-butyl-2-(N-phenylpiperazinyl-N'-methyl)phenoxo)zinc]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[ethyl(μ-4,6-di-tert-butyl-2-(N-phenylpiperazinyl-N'-methyl)phenoxo)zinc]

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Technology Process of bis[ethyl(μ-4,6-di-tert-butyl-2-(N-phenylpiperazinyl-N'-methyl)phenoxo)zinc]

There total 1 articles about bis[ethyl(μ-4,6-di-tert-butyl-2-(N-phenylpiperazinyl-N'-methyl)phenoxo)zinc] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 874750-72-8
2-(N-phenylpiperazinyl-N'-methyl)-4,6-di-tert-butyl-phenol

: 557-20-0
diethylzinc

: 874750-74-0
bis[ethyl(μ-4,6-di-tert-butyl-2-(N-phenylpiperazinyl-N'-methyl)phenoxo)zinc]

Guidance literature:: In diethyl ether; under Ar; ZnEt2 in Et2O added dropwise to soln. of ligand in Et2O at -35°C; warmed with stirring to ambient temp. for 16 h; filtered; ppt. washed with hexane; extd. into THF-hexane; extract concd.in vac.; crystd. at -25°C; elem. anal.;
DOI:10.1016/j.jorganchem.2008.02.012

Reference yield: 94.0%

: 874750-74-0
bis[ethyl(μ-4,6-di-tert-butyl-2-(N-phenylpiperazinyl-N'-methyl)phenoxo)zinc]

: 1031358-20-9
bis[4,6-di-tert-butyl-2-(N-phenylpiperazinyl-N'-methyl)phenoxo]zinc

Guidance literature:: With methanol; In tetrahydrofuran; hexane; byproducts: C2H6; under Ar; MeOH (2 equiv.) in hexane added dropwise to stirred soln. of Zn complex in THF-hexane at -78°C; warmed to ambient temp. over 4 h; volatiles removed in vac.; extd. with THF-hexane; extract concd.; crystd. at 0°C; elem. anal.;
DOI:10.1016/j.jorganchem.2008.02.012