C₂₆H₂₈N₂O₄

Base Information

Chemical Name:C₂₆H₂₈N₂O₄
CAS No.:1253798-68-3
Molecular Formula:C₂₆H₂₈N₂O₄
Molecular Weight:432.519
Hs Code.:

C<sub>26</sub>H<sub>28</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₆H₂₈N₂O₄

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Chemical Property of C₂₆H₂₈N₂O₄

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Technology Process of C₂₆H₂₈N₂O₄

There total 5 articles about C₂₆H₂₈N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1253798-67-2
phenyl 3-benzyloxy-5-(dimethylaminomethyl)isoxazole-4-carboxylate

: 194410-40-7
(1R,4S,4aR,8aS)-7-Methyl-4,4a,8,8a-tetrahydro-1H-1,4-methano-naphthalen-5-one

: 1253798-68-3
C₂₆H₂₈N₂O₄

Guidance literature:: phenyl 3-benzyloxy-5-(dimethylaminomethyl)isoxazole-4-carboxylate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - -20 ℃; Inert atmosphere;

(1R,4S,4aR,8aS)-7-Methyl-4,4a,8,8a-tetrahydro-1H-1,4-methano-naphthalen-5-one; In tetrahydrofuran; at -78 - -23 ℃; Inert atmosphere;

Reference yield:

: 51175-59-8
norbornenoquinone

: 1253798-68-3
C₂₆H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 3 h / 5 - 23 °C / Inert atmosphere

2.1: triethylamine / Immobilised Lipase PS "Amino" / 22 h / 23 °C / Inert atmosphere

3.1: ammonium formate / bis-triphenylphosphine-palladium(II) chloride / acetonitrile / 0.33 h / 100 - 105 °C / Inert atmosphere

4.1: N,N,N,N,N,N-hexamethylphosphoric triamide; chloro-trimethyl-silane / tetrahydrofuran / Inert atmosphere

4.2: 0.33 h / -78 °C / Inert atmosphere

4.3: 23 h / 20 °C

5.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 - -20 °C / Inert atmosphere

5.2: -78 - -23 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; chloro-trimethyl-silane; cerium(III) chloride heptahydrate; ammonium formate; triethylamine; lithium hexamethyldisilazane; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; methanol; acetonitrile; 5.1: Michael Claisen Condensation;

Reference yield:

: 678197-26-7
tricyclo[6.2.1.0^2,7]undeca-4,9-diene-3,6-diol

: 1253798-68-3
C₂₆H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / Immobilised Lipase PS "Amino" / 22 h / 23 °C / Inert atmosphere

2.1: ammonium formate / bis-triphenylphosphine-palladium(II) chloride / acetonitrile / 0.33 h / 100 - 105 °C / Inert atmosphere

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; chloro-trimethyl-silane / tetrahydrofuran / Inert atmosphere

3.2: 0.33 h / -78 °C / Inert atmosphere

3.3: 23 h / 20 °C

4.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 - -20 °C / Inert atmosphere

4.2: -78 - -23 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; chloro-trimethyl-silane; ammonium formate; triethylamine; lithium hexamethyldisilazane; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; acetonitrile; 4.1: Michael Claisen Condensation;