4-O-Benzyl-1-(benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-L-xylo-tetritol

Base Information

Chemical Name:4-O-Benzyl-1-(benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-L-xylo-tetritol
CAS No.:173382-31-5
Molecular Formula:C₂₅H₂₈N₂O₅S
Molecular Weight:468.574
Hs Code.:

Synonyms:4-O-Benzyl-1-(benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-L-xylo-tetritol

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Chemical Property of 4-O-Benzyl-1-(benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-L-xylo-tetritol

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Technology Process of 4-O-Benzyl-1-(benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-L-xylo-tetritol

There total 3 articles about 4-O-Benzyl-1-(benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-L-xylo-tetritol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: C-[(S)-C-((4S,5S)-5-Benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-C-thiazol-2-yl]-methylamine

: 173382-31-5
4-O-Benzyl-1-(benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-L-xylo-tetritol

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; at 0 ℃; for 0.333333h; Yield given;

Reference yield:

: 152390-96-0,885500-75-4
(Z)-N-(4-O-benzyl-1-deoxy-2,3-O-isopropylidene-L-ylidene)benzylamine-N-oxide

: 173382-31-5
4-O-Benzyl-1-(benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-L-xylo-tetritol

Guidance literature:: Multi-step reaction with 3 steps

1: BuLi, Et₂AlCl / diethyl ether; hexane / 1.) -78 deg C, 15 min, 2.) -80 deg C, 30 min

2: 20percent aq. TiCl₃ / methanol / 0.25 h / Ambient temperature

3: 7percent aq. NaHCO₃ / dioxane / 0.33 h / 0 °C

With n-butyllithium; titanium(III) chloride; diethylaluminium chloride; sodium hydrogencarbonate; In 1,4-dioxane; methanol; diethyl ether; hexane;

Reference yield:

: 173382-54-2
N-Benzyl-4-O-benzyl-1-deoxy-1-(hydroxyamino)-2,3-O-isopropylidene-1-(2-thiazolyl)-L-xylo-tetritol

: 173382-31-5
4-O-Benzyl-1-(benzyloxycarbonylamino)-1-deoxy-2,3-O-isopropylidene-1-(2-thiazolyl)-L-xylo-tetritol

Guidance literature:: Multi-step reaction with 2 steps

1: 20percent aq. TiCl₃ / methanol / 0.25 h / Ambient temperature

2: 7percent aq. NaHCO₃ / dioxane / 0.33 h / 0 °C

With titanium(III) chloride; sodium hydrogencarbonate; In 1,4-dioxane; methanol;