2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranosyl trichloroacetimidate

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranosyl trichloroacetimidate
CAS No.:1245641-31-9
Molecular Formula:C₃₆H₃₈Cl₃NO₁₆
Molecular Weight:847.054
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranosyl trichloroacetimidate

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Chemical Property of 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranosyl trichloroacetimidate

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Technology Process of 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranosyl trichloroacetimidate

There total 1 articles about 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranose

: 545-06-2
trichloroacetonitrile

: 1245641-31-9
2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1248/cpb.58.495

Reference yield: 84.0%

: 1892-29-1
bis(2-hydroxyethyl) disulfide

: 1245641-31-9
2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranosyl trichloroacetimidate

: 1355150-70-7
bis(2-ethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-β-L-fucopyranoside) disulfide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h; stereoselective reaction; Molecular sieve;
DOI:10.1248/cpb.59.1307

Reference yield: 70.0%

: 1245641-31-9
2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranosyl trichloroacetimidate

: 1355150-67-2
2,3,4,5-tetra-O-acetyl-1-azido-1-deoxy-D-mannitol

: 1355150-68-3
2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-β-L-fucopyranosyl-(1->6)-2,3,4,5-tetra-O-acetyl-1-deoxy-1-azido-D-mannitol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h; Molecular sieve;
DOI:10.1248/cpb.59.1307