3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol

Base Information

• Chemical Name: 3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol
• CAS No.: 911701-85-4
• Molecular Formula: C₃₂H₂₈F₆O₄
• Molecular Weight: 590.562

Synonyms:3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol

Chemical Property of 3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol

Chemical Property:

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Technology Process of 3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol

There total 2 articles about 3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxy diphenate dimethyl ester (911701-84-3) → (R)-3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol (911701-85-4) + (S)-3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol (911701-85-4)

Guidance literature:

3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxy diphenate dimethyl ester; With lithium aluminium tetrahydride; In cyclopentyl methyl ether; at -10 - 0 ℃; for 3h;

With hydrogenchloride; In cyclopentyl methyl ether; water;

Reference yield:

3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxy diphenate dimethyl ester (911701-84-3) → (R)-3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol (911701-85-4) + (S)-3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol (911701-85-4)

Guidance literature:

3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxy diphenate dimethyl ester; With lithium aluminium tetrahydride; In cyclopentyl methyl ether; at -10 - 0 ℃; for 3h;

With hydrogenchloride; In cyclopentyl methyl ether; water;

Reference yield:

3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethanol (911701-85-4) → (R)-3,3'-bis(3,4,5,-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethyl bromide + (S)-3,3'-bis(3,4,5,-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxybiphenyl-2,2'-dimethyl bromide

Guidance literature:

With phosphorus tribromide; In cyclopentyl methyl ether; at 0 ℃; for 4h;

upstream raw materials:

3,3'-bis(3,4,5-trifluorophenyl)-4,6,4',6'-tetramethyl-5,5'-dimethoxy diphenate dimethyl ester

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