(R)-N,N-dimethyl-1-[1-(4-chlorophenyl)cyclobutyl]-3-methylbutylamine hydrogensulfate

Base Information

• Chemical Name: (R)-N,N-dimethyl-1-[1-(4-chlorophenyl)cyclobutyl]-3-methylbutylamine hydrogensulfate
• CAS No.: 1238593-23-1
• Molecular Formula: C₁₇H₂₆ClN*H₂O₄S
• Molecular Weight: 377.933

Synonyms:(R)-N,N-dimethyl-1-[1-(4-chlorophenyl)cyclobutyl]-3-methylbutylamine hydrogensulfate

Chemical Property of (R)-N,N-dimethyl-1-[1-(4-chlorophenyl)cyclobutyl]-3-methylbutylamine hydrogensulfate

Chemical Property:

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Technology Process of (R)-N,N-dimethyl-1-[1-(4-chlorophenyl)cyclobutyl]-3-methylbutylamine hydrogensulfate

There total 2 articles about (R)-N,N-dimethyl-1-[1-(4-chlorophenyl)cyclobutyl]-3-methylbutylamine hydrogensulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.3%

(R)-N,N-dimethyl-1-[1-(4-chlorophenyl)cyclobutyl]-3-methylbutylamine D-tartrate → (R)-N,N-dimethyl-1-[1-(4-chlorophenyl)cyclobutyl]-3-methylbutylamine hydrogensulfate (1238593-23-1)

Guidance literature:

(R)-N,N-dimethyl-1-[1-(4-chlorophenyl)cyclobutyl]-3-methylbutylamine D-tartrate; With potassium carbonate; In chloroform; water; at 20 ℃; for 0.5h;

With sulfuric acid; In chloroform; at 20 ℃;

Reference yield: 71.2%

sibutramine (106650-56-0) → (R)-N,N-dimethyl-1-[1-(4-chlorophenyl)cyclobutyl]-3-methylbutylamine hydrogensulfate (1238593-23-1)

Guidance literature:

sibutramine; With L-Tartaric acid; In methanol; ethyl acetate; at 20 - 60 ℃; for 25h; Resolution of racemate;

With potassium carbonate; In methanol; water; ethyl acetate; at 20 ℃; for 0.5h; Resolution of racemate;

With sulfuric acid; In methanol; ethyl acetate; at 20 ℃; for 18.1667h; Resolution of racemate;

upstream raw materials:

sibutramine

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