Technology Process of C23H25N3
There total 3 articles about C23H25N3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triphenylphosphine; cesium fluoride; palladium dichloride;
In
ethanol; water; toluene;
at 80 ℃;
for 18h;
Schlenk technique;
Inert atmosphere;
DOI:10.1039/c3cc48017h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate; trimethylsilylazide; N-iodo-succinimide / dichloromethane; water / 0 - 30 °C / Schlenk technique; Inert atmosphere
2: sodium L-ascorbate; copper(ll) sulfate pentahydrate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / N,N-dimethyl-formamide / 1 h / 70 °C / Microwave irradiation; Inert atmosphere
3: palladium dichloride; triphenylphosphine; cesium fluoride / toluene; water; ethanol / 18 h / 80 °C / Schlenk technique; Inert atmosphere
With
N-iodo-succinimide; copper(ll) sulfate pentahydrate; (triphenylphosphine)gold(I) chloride; trimethylsilylazide; silver trifluoromethanesulfonate; sodium L-ascorbate; triphenylphosphine; cesium fluoride; palladium dichloride; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
3: |Suzuki-Miyaura Coupling;
DOI:10.1039/c3cc48017h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium L-ascorbate; copper(ll) sulfate pentahydrate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / N,N-dimethyl-formamide / 1 h / 70 °C / Microwave irradiation; Inert atmosphere
2: palladium dichloride; triphenylphosphine; cesium fluoride / toluene; water; ethanol / 18 h / 80 °C / Schlenk technique; Inert atmosphere
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate; triphenylphosphine; cesium fluoride; palladium dichloride; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
ethanol; water; N,N-dimethyl-formamide; toluene;
2: |Suzuki-Miyaura Coupling;
DOI:10.1039/c3cc48017h