4-amino-6,7-dimethyl-2-oxo-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,3-dihydropteridine

Base Information

Chemical Name:4-amino-6,7-dimethyl-2-oxo-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,3-dihydropteridine
CAS No.:312602-48-5
Molecular Formula:C₃₄H₂₉N₅O₈
Molecular Weight:635.633
Hs Code.:

Synonyms:4-amino-6,7-dimethyl-2-oxo-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,3-dihydropteridine

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Chemical Property of 4-amino-6,7-dimethyl-2-oxo-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,3-dihydropteridine

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Technology Process of 4-amino-6,7-dimethyl-2-oxo-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,3-dihydropteridine

There total 5 articles about 4-amino-6,7-dimethyl-2-oxo-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,3-dihydropteridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 431-03-8
dimethylglyoxal

: 312602-10-1
5,6-diamino-2',3',5'-tri-O-benzoylcytidine

: 312602-54-3
C₃₄H₂₉N₅O₈

: 312602-48-5
4-amino-6,7-dimethyl-2-oxo-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,3-dihydropteridine

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1021/ol0064765

Reference yield:

: 312602-05-4
6-amino-2',3',5'-tri-O-benzoylcytidine

: 312602-48-5
4-amino-6,7-dimethyl-2-oxo-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,3-dihydropteridine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NaNO₂ / acetic acid; H₂O / 4 h / cooling

2: 97.5 percent / Na₂S₂O₄ / dimethylformamide; H₂O / 4 h / 50 °C

3: 83 percent / dimethylformamide / 1 h / 20 °C

With sodium dithionite; sodium nitrite; In water; acetic acid; N,N-dimethyl-formamide; 1: Nitrosation / 2: Reduction / 3: cyclocondensation;
DOI:10.1021/ol0064765

Reference yield:

: 312602-08-7
6-amino-5-nitroso-2',3',5'-tri-O-benzoylcytidine

: 312602-48-5
4-amino-6,7-dimethyl-2-oxo-3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2,3-dihydropteridine

Guidance literature:: Multi-step reaction with 2 steps

1: 97.5 percent / Na₂S₂O₄ / dimethylformamide; H₂O / 4 h / 50 °C

2: 83 percent / dimethylformamide / 1 h / 20 °C

With sodium dithionite; In water; N,N-dimethyl-formamide; 1: Reduction / 2: cyclocondensation;
DOI:10.1021/ol0064765