tris(4-tert-butylphenyl)acetyl chloride

Base Information

Chemical Name:tris(4-tert-butylphenyl)acetyl chloride
CAS No.:1417038-27-7
Molecular Formula:C₃₂H₃₉ClO
Molecular Weight:475.114
Hs Code.:

Synonyms:tris(4-tert-butylphenyl)acetyl chloride

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Chemical Property of tris(4-tert-butylphenyl)acetyl chloride

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Technology Process of tris(4-tert-butylphenyl)acetyl chloride

There total 2 articles about tris(4-tert-butylphenyl)acetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tris(4-tert-butylphenyl)acetic acid

: 1417038-27-7
tris(4-tert-butylphenyl)acetyl chloride

Guidance literature:: With thionyl chloride; at 80 ℃; for 1.5h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ic302149p

Reference yield:

: 27541-51-1
tris(4-(tert-butyl))phenylmethane

: 1417038-27-7
tris(4-tert-butylphenyl)acetyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium; carbon dioxide / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane / 2.5 h / -70 - -30 °C / Inert atmosphere; Schlenk technique

2: thionyl chloride / 1.5 h / 80 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; thionyl chloride; carbon dioxide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane;
DOI:10.1021/ic302149p