2'-(CH₂OCH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine 9-carboxylate

Base Information

Chemical Name:2'-(CH₂OCH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine 9-carboxylate
CAS No.:1031363-95-7
Molecular Formula:C₂₇H₂₅NO₆
Molecular Weight:459.499
Hs Code.:

2'-(CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine 9-carboxylate

Synonyms:2'-(CH₂OCH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine 9-carboxylate

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Chemical Property of 2'-(CH₂OCH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine 9-carboxylate

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Technology Process of 2'-(CH₂OCH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine 9-carboxylate

There total 5 articles about 2'-(CH₂OCH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine 9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 5336-90-3
acridine-9-carboxylic acid

: 1031363-93-5
methyl 3-(CH₂OCH₂CH₂OMe)-4-hydroxy-5-methylbenzoate

: 1031363-95-7
2'-(CH₂OCH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine 9-carboxylate

Guidance literature:: acridine-9-carboxylic acid; With pyridine; p-toluenesulfonyl chloride; for 0.166667h;

methyl 3-(CH₂OCH₂CH₂OMe)-4-hydroxy-5-methylbenzoate; at 20 ℃; for 96h; Inert atmosphere;

Reference yield:

: 4919-37-3
3,5-dimethyl-4-hydroxybenzoic acid

: 1031363-95-7
2'-(CH₂OCH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine 9-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / 20 °C / Cooling with ice

2.1: pyridine / 0 - 20 °C / Inert atmosphere

3.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 6 h / Reflux; Inert atmosphere

4.1: sodium hydrogencarbonate / 2 h / 90 - 95 °C / Inert atmosphere

5.1: pyridine; p-toluenesulfonyl chloride / 0.17 h

5.2: 96 h / 20 °C / Inert atmosphere

With pyridine; N-Bromosuccinimide; thionyl chloride; 2,2'-azobis(isobutyronitrile); sodium hydrogencarbonate; p-toluenesulfonyl chloride; In tetrachloromethane;

Reference yield:

: 1031363-89-9
1-acetoxy-4-methoxycarbonyl-2,6-dimethylbenzene

: 1031363-95-7
2'-(CH₂OCH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine 9-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 6 h / Reflux; Inert atmosphere

2.1: sodium hydrogencarbonate / 2 h / 90 - 95 °C / Inert atmosphere

3.1: pyridine; p-toluenesulfonyl chloride / 0.17 h

3.2: 96 h / 20 °C / Inert atmosphere

With pyridine; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydrogencarbonate; p-toluenesulfonyl chloride; In tetrachloromethane;