Benzyl-naphthalen-1-yl-carbodiimide

Base Information

• Chemical Name: Benzyl-naphthalen-1-yl-carbodiimide
• CAS No.: 130412-95-2
• Molecular Formula: C₁₈H₁₄N₂
• Molecular Weight: 258.323
• Mol file: 130412-95-2.mol

Synonyms:Benzyl-naphthalen-1-yl-carbodiimide

Chemical Property of Benzyl-naphthalen-1-yl-carbodiimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzyl-naphthalen-1-yl-carbodiimide

There total 5 articles about Benzyl-naphthalen-1-yl-carbodiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzyl-3-(naphthalen-1-yl)thiourea (107544-71-8) → Benzyl-naphthalen-1-yl-carbodiimide (130412-95-2)

Guidance literature:

1-benzyl-3-(naphthalen-1-yl)thiourea; With methyl iodide; In ethanol; dichloromethane; at 23 ℃; for 48h;

With silver nitrate; triethylamine; In dichloromethane; acetonitrile; at 23 ℃; for 48h;

Reference yield:

C19H18N2S → Benzyl-naphthalen-1-yl-carbodiimide (130412-95-2)

Guidance literature:

With silver nitrate; triethylamine; In acetonitrile; at 0 - 23 ℃; for 2h;

DOI:10.1021/acs.joc.1c01281

Reference yield:

1-amino-naphthalene (134-32-7) → Benzyl-naphthalen-1-yl-carbodiimide (130412-95-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: dichloromethane / 24 h / 23 °C

2.1: methyl iodide / ethanol; dichloromethane / 48 h / 23 °C

2.2: 48 h / 23 °C

With methyl iodide; In ethanol; dichloromethane;

upstream raw materials:

1-<<(Triphenylphosphoranylidene)amino>methyl>benzotriazole

1-Naphthyl isocyanate

Benzyl isothiocyanate

1-amino-naphthalene

Refernces

• 1、 -. "Pos [...] 4 group metal olefin polymerization catalyst". . . Retrieved 2019/08/27.