methyl 6-((1S,2R,6S)-2-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-1-hydroxy-6-methyloctyl)phenazine-1-carboxylate

Base Information

Chemical Name:methyl 6-((1S,2R,6S)-2-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-1-hydroxy-6-methyloctyl)phenazine-1-carboxylate
CAS No.:1369415-68-8
Molecular Formula:C₃₄H₃₇N₃O₆
Molecular Weight:583.684
Hs Code.:

Synonyms:methyl 6-((1S,2R,6S)-2-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-1-hydroxy-6-methyloctyl)phenazine-1-carboxylate

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Chemical Property of methyl 6-((1S,2R,6S)-2-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-1-hydroxy-6-methyloctyl)phenazine-1-carboxylate

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Technology Process of methyl 6-((1S,2R,6S)-2-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-1-hydroxy-6-methyloctyl)phenazine-1-carboxylate

There total 4 articles about methyl 6-((1S,2R,6S)-2-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-1-hydroxy-6-methyloctyl)phenazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1336882-47-3
methyl 6-formylphenazine-1-carboxylate

: 1369415-67-7
(S)-4-benzyl-3-((S)-6-methyloctanoyl)oxazolidin-2-one

: 1369415-68-8
methyl 6-((1S,2R,6S)-2-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-1-hydroxy-6-methyloctyl)phenazine-1-carboxylate

Guidance literature:: (S)-4-benzyl-3-((S)-6-methyloctanoyl)oxazolidin-2-one; With triethylamine; magnesium chloride; In ethyl acetate; at 20 ℃; for 0.166667h;

methyl 6-formylphenazine-1-carboxylate; With chloro-trimethyl-silane; In ethyl acetate; at 20 ℃;
DOI:10.1021/jo202642a

Reference yield:

: 504-99-4,928-30-3,97749-11-6,150950-00-8
(6S)-6-methyloctanoic acid

: 1369415-68-8
methyl 6-((1S,2R,6S)-2-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-1-hydroxy-6-methyloctyl)phenazine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C

2.2: -78 - 20 °C

3.1: triethylamine; magnesium chloride / ethyl acetate / 0.17 h / 20 °C

3.2: 20 °C

With n-butyllithium; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; magnesium chloride; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate;
DOI:10.1021/jo202642a

Reference yield:

: 110453-78-6
(S)-(+)-6-methyl-1-octanol

: 1369415-68-8
methyl 6-((1S,2R,6S)-2-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-1-hydroxy-6-methyloctyl)phenazine-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium dihydrogenphosphate; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; acetonitrile / 16 h / 20 °C

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 0 - 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C

3.2: -78 - 20 °C

4.1: triethylamine; magnesium chloride / ethyl acetate / 0.17 h / 20 °C

4.2: 20 °C

With sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; triethylamine; N,N-dimethyl-formamide; magnesium chloride; In tetrahydrofuran; hexane; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1021/jo202642a