(E)-N-(3-(2-(3-chlorobenzyl)-2H-tetrazol-5-yl)phenyl)-2-m-tolylethenesulfonamide

Base Information

Chemical Name:(E)-N-(3-(2-(3-chlorobenzyl)-2H-tetrazol-5-yl)phenyl)-2-m-tolylethenesulfonamide
CAS No.:1333394-08-3
Molecular Formula:C₂₃H₂₀ClN₅O₂S
Molecular Weight:465.963
Hs Code.:

Synonyms:(E)-N-(3-(2-(3-chlorobenzyl)-2H-tetrazol-5-yl)phenyl)-2-m-tolylethenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(3-(2-(3-chlorobenzyl)-2H-tetrazol-5-yl)phenyl)-2-m-tolylethenesulfonamide

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Technology Process of (E)-N-(3-(2-(3-chlorobenzyl)-2H-tetrazol-5-yl)phenyl)-2-m-tolylethenesulfonamide

There total 5 articles about (E)-N-(3-(2-(3-chlorobenzyl)-2H-tetrazol-5-yl)phenyl)-2-m-tolylethenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1333393-90-0
3-(2-(3-chlorobenzyl)-2H-tetrazol-5-yl)aniline

: (E)-2-m-tolylethenesulfonyl chloride

: 1333394-08-3
(E)-N-(3-(2-(3-chlorobenzyl)-2H-tetrazol-5-yl)phenyl)-2-m-tolylethenesulfonamide

Guidance literature:: With sodium carbonate; In tetrahydrofuran; water; at 20 ℃; for 5h;
DOI:10.1016/j.bmcl.2011.07.023

Reference yield:

: 1333394-16-3
2-(3-chlorobenzyl)-5-(3-nitrophenyl)-2H-tetrazole

: 1333394-08-3
(E)-N-(3-(2-(3-chlorobenzyl)-2H-tetrazol-5-yl)phenyl)-2-m-tolylethenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; zinc / 2.5 h / 20 °C

2: sodium carbonate / tetrahydrofuran; water / 5 h / 20 °C

With sodium carbonate; acetic acid; zinc; In tetrahydrofuran; water;
DOI:10.1016/j.bmcl.2011.07.023

Reference yield:

: 100-80-1
3-methylstyrene

: 1333394-08-3
(E)-N-(3-(2-(3-chlorobenzyl)-2H-tetrazol-5-yl)phenyl)-2-m-tolylethenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl dichloride / N,N-dimethyl-formamide / 7 h / 75 °C

2: sodium carbonate / tetrahydrofuran; water / 5 h / 20 °C

With sulfuryl dichloride; sodium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.07.023