Methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-(methanesulfonyl)-α-D-glucopyranoside

Base Information

Chemical Name:Methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-(methanesulfonyl)-α-D-glucopyranoside
CAS No.:147425-48-7
Molecular Formula:C₂₂H₂₆O₈S
Molecular Weight:450.51
Hs Code.:

Synonyms:Methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-(methanesulfonyl)-α-D-glucopyranoside

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Chemical Property of Methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-(methanesulfonyl)-α-D-glucopyranoside

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Technology Process of Methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-(methanesulfonyl)-α-D-glucopyranoside

There total 10 articles about Methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-(methanesulfonyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 158548-92-6
Methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-6-iodo-4-O-(methanesulfonyl)-α-D-glucopyranoside

: 147425-48-7
Methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-(methanesulfonyl)-α-D-glucopyranoside

Guidance literature:: With acetic acid; zinc; In diethyl ether; for 5h;
DOI:10.1021/jo00094a040

Reference yield:

: 147425-47-6
Methyl 3-O-benzoyl-2-O-benzyl-4,6-bis-O-(methanesulfonyl)-α-D-glucopyranoside

: 147425-48-7
Methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-(methanesulfonyl)-α-D-glucopyranoside

Guidance literature:: With acetic acid; sodium iodide; zinc; Yield given. Multistep reaction; 1) EtCOMe, reflux, 2) ether, rt;
DOI:10.1016/0040-4039(93)85088-E

Reference yield:

: 76375-66-1
methyl 2-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

: 147425-48-7
Methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-(methanesulfonyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / pyridine / 1.) 0 deg C to r.t., 2.) r.t., 4 h

2: 94 percent / CF₃COOH / methanol; H₂O / 20 h / Ambient temperature

3: 92 percent / pyridine / 12 h / 3 °C

4: 94 percent / NaI / butan-2-one / 2 h / Heating

5: 91 percent / Zn, glacial CH₃COOH / diethyl ether / 5 h

With pyridine; acetic acid; trifluoroacetic acid; sodium iodide; zinc; In methanol; diethyl ether; water; butanone;
DOI:10.1021/jo00094a040