15,15-dioxo-2-phenyl-tetrahydro-15λ⁶-5r,10c-ethano-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione

Base Information

• Chemical Name: 15,15-dioxo-2-phenyl-tetrahydro-15λ⁶-5r,10c-ethano-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione
• CAS No.: 64776-61-0
• Molecular Formula: C₂₀H₂₃N₃O₄S
• Molecular Weight: 401.486

Synonyms:15,15-dioxo-2-phenyl-tetrahydro-15λ⁶-5r,10c-ethano-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione

Chemical Property of 15,15-dioxo-2-phenyl-tetrahydro-15λ⁶-5r,10c-ethano-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of 15,15-dioxo-2-phenyl-tetrahydro-15λ⁶-5r,10c-ethano-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione

There total 9 articles about 15,15-dioxo-2-phenyl-tetrahydro-15λ⁶-5r,10c-ethano-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) → 15,15-dioxo-2-phenyl-tetrahydro-15λ6-5r,10c-ethano-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione (64776-61-0)

Guidance literature:

Multi-step reaction with 3 steps

1: CH₂Cl₂

2: MCPBA / CH₂Cl₂

3: H₂ / PtO₂ / ethyl acetate

With hydrogen; 3-chloro-benzenecarboperoxoic acid; platinum(IV) oxide; In dichloromethane; ethyl acetate;

DOI:10.1016/0040-4020(77)80411-0

Reference yield:

15,15-dioxo-2-phenyl-tetrahydro-15λ6-5r,10c-etheno-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione (64776-65-4) → 15,15-dioxo-2-phenyl-tetrahydro-15λ6-5r,10c-ethano-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione (64776-61-0)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethyl acetate;

DOI:10.1016/0040-4020(77)80411-0

Reference yield:

15,15-dioxo-2-phenyl-15λ6-5r,10c-etheno-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione (64776-53-0,64812-90-4) → 15,15-dioxo-2-phenyl-tetrahydro-15λ6-5r,10c-ethano-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione (64776-61-0)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethyl acetate;

DOI:10.1016/0040-4020(77)80411-0

upstream raw materials:

15,15-dioxo-2-phenyl-tetrahydro-15λ⁶-5r,10c-etheno-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione

15,15-dioxo-2-phenyl-15λ⁶-5r,10c-etheno-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione

4-Phenyl-1,2,4-triazolidine-3,5-dione

12-thia-[4.4.3]propella-2,4-diene

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