methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate

Base Information

Chemical Name:methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate
CAS No.:1093345-94-8
Molecular Formula:C₂₈H₃₁NO₁₀S
Molecular Weight:573.621
Hs Code.:

Synonyms:methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate

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Chemical Property of methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate

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Technology Process of methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate

There total 1 articles about methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 898224-36-7
methyl (phenyl 5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate

: 108-24-7
acetic anhydride

: 1093345-94-8
methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ol802207e

Reference yield: 77.0%

: 111-87-5
octanol

: 1093345-94-8
methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate

: 1159168-12-3
C₃₀H₄₃NO₁₁

Guidance literature:: octanol; methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate; With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -35 ℃; for 5h; Molecular sieve; Inert atmosphere;

With triethylamine; In dichloromethane; optical yield given as %de;
DOI:10.1021/jo900176e

Reference yield: 56.0%

: 1093345-94-8
methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate

: potassium salt of 2-mercaptobenzoxazole

: 1093345-86-8
methyl (benzoxazol-2yl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Guidance literature:: methyl (phenyl 7,8-di-O-acetyl-5-amino-9-O-benzyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-2-nonulopyranosid)onate; With Iodine monochloride; In dichloromethane; at 0 ℃; for 3h; Molecular sieve;

potassium salt of 2-mercaptobenzoxazole; With 18-crown-6 ether; In acetone; at 20 ℃; for 24h;
DOI:10.1021/ol802207e