(Z)-N-(tert-butoxycarbonyl)-β-(dibenzothien-4-yl)dehydrophenylalanine methyl ester

Base Information

Chemical Name:(Z)-N-(tert-butoxycarbonyl)-β-(dibenzothien-4-yl)dehydrophenylalanine methyl ester
CAS No.:1037600-87-5
Molecular Formula:C₂₇H₂₅NO₄S
Molecular Weight:459.566
Hs Code.:

Synonyms:(Z)-N-(tert-butoxycarbonyl)-β-(dibenzothien-4-yl)dehydrophenylalanine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N-(tert-butoxycarbonyl)-β-(dibenzothien-4-yl)dehydrophenylalanine methyl ester

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Technology Process of (Z)-N-(tert-butoxycarbonyl)-β-(dibenzothien-4-yl)dehydrophenylalanine methyl ester

There total 1 articles about (Z)-N-(tert-butoxycarbonyl)-β-(dibenzothien-4-yl)dehydrophenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 108847-20-7
4-dibenzothiophene boronic acid

: 606937-28-4
Boc-(Z)-ΔPhe(β-Br)-OMe

: 1037600-87-5
(Z)-N-(tert-butoxycarbonyl)-β-(dibenzothien-4-yl)dehydrophenylalanine methyl ester

Guidance literature:: With caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; water; at 70 - 80 ℃; for 1.5h;
DOI:10.1016/j.bmc.2008.04.004

Reference yield: 37.0%

: 1037600-87-5
(Z)-N-(tert-butoxycarbonyl)-β-(dibenzothien-4-yl)dehydrophenylalanine methyl ester

: 1037600-84-2
C₂₂H₁₅NO₂S

: 1037600-83-1
C₂₂H₁₅NO₂S

Guidance literature:: With copper diacetate; palladium diacetate; In N,N-dimethyl-formamide; at 130 - 160 ℃; for 7h;
DOI:10.1016/j.bmc.2008.04.004