2-Azido-3-formylthiophene

Base Information

• Chemical Name: 2-Azido-3-formylthiophene
• CAS No.: 163079-30-9
• Molecular Formula: C₅H₃N₃OS
• Molecular Weight: 153.164
• Mol file: 163079-30-9.mol

Synonyms:2-Azido-3-formylthiophene

Chemical Property of 2-Azido-3-formylthiophene

Chemical Property:

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Technology Process of 2-Azido-3-formylthiophene

There total 1 articles about 2-Azido-3-formylthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2-nitro-3-thiophenecarbaldehyde (41057-04-9) → 2-Azido-3-formylthiophene (163079-30-9)

Guidance literature:

With sodium azide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 0 ℃; for 0.5h;

DOI:10.1021/jo00112a054

Reference yield: 50.0%

2-Azido-3-formylthiophene (163079-30-9) → 2-amino-3-thiophenecarbaldhyde (40341-23-9)

Guidance literature:

With hexamethyldisilathiane; In methanol; for 0.5h; Ambient temperature;

DOI:10.1021/jo00112a054

upstream raw materials:

2-nitro-3-thiophenecarbaldehyde

Downstream raw materials:

2-amino-3-thiophenecarbaldhyde