2-chloro-7-methyl-8-(3-methylbutyl)-5-phenyl-7,8-dihydropteridin-6(5H)-one

Base Information

Chemical Name:2-chloro-7-methyl-8-(3-methylbutyl)-5-phenyl-7,8-dihydropteridin-6(5H)-one
CAS No.:1435462-62-6
Molecular Formula:C₁₈H₂₁ClN₄O
Molecular Weight:344.844
Hs Code.:

Synonyms:2-chloro-7-methyl-8-(3-methylbutyl)-5-phenyl-7,8-dihydropteridin-6(5H)-one

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Chemical Property of 2-chloro-7-methyl-8-(3-methylbutyl)-5-phenyl-7,8-dihydropteridin-6(5H)-one

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Technology Process of 2-chloro-7-methyl-8-(3-methylbutyl)-5-phenyl-7,8-dihydropteridin-6(5H)-one

There total 4 articles about 2-chloro-7-methyl-8-(3-methylbutyl)-5-phenyl-7,8-dihydropteridin-6(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 501439-14-1
2-chloro-7-methyl-8-(3-methylbutyl)-7,8-dihydropteridin-6(5H)-one

: 98-80-6
phenylboronic acid

: 1435462-62-6
2-chloro-7-methyl-8-(3-methylbutyl)-5-phenyl-7,8-dihydropteridin-6(5H)-one

Guidance literature:: With oxygen; copper diacetate; triethylamine; In dichloromethane; at 20 ℃; for 48h; Molecular sieve;

Reference yield:

: 1435462-61-5
methyl N-(2-chloro-5-nitropyrimidin-4-yl)-N-(3-methylbutyl)alaninate

: 1435462-62-6
2-chloro-7-methyl-8-(3-methylbutyl)-5-phenyl-7,8-dihydropteridin-6(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: iron; acetic acid / 2 h / 60 °C

2: oxygen; copper diacetate; triethylamine / dichloromethane / 48 h / 20 °C / Molecular sieve

With oxygen; copper diacetate; iron; acetic acid; triethylamine; In dichloromethane;

Reference yield:

: 1435462-60-4
methyl N-(3-methylbutyl)alaninate

: 1435462-62-6
2-chloro-7-methyl-8-(3-methylbutyl)-5-phenyl-7,8-dihydropteridin-6(5H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydrogencarbonate / water; diethyl ether / 2 h / -10 - 20 °C

2: iron; acetic acid / 2 h / 60 °C

3: oxygen; copper diacetate; triethylamine / dichloromethane / 48 h / 20 °C / Molecular sieve

With oxygen; copper diacetate; iron; potassium hydrogencarbonate; acetic acid; triethylamine; In diethyl ether; dichloromethane; water;