3-bromo-7,8,9,10-tetraphenylfluoranthene

Base Information

• Chemical Name: 3-bromo-7,8,9,10-tetraphenylfluoranthene
• CAS No.: 96765-93-4
• Molecular Formula: C₄₀H₂₅Br
• Molecular Weight: 585.543
• Mol file: 96765-93-4.mol

Synonyms:3-bromo-7,8,9,10-tetraphenylfluoranthene

Chemical Property of 3-bromo-7,8,9,10-tetraphenylfluoranthene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-bromo-7,8,9,10-tetraphenylfluoranthene

There total 3 articles about 3-bromo-7,8,9,10-tetraphenylfluoranthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

3-bromo-7,9-diphenyl-8H-cyclopenta[a]acenaphthylen-8-one + diphenyl acetylene (501-65-5) → 3-bromo-7,8,9,10-tetraphenylfluoranthene (96765-93-4)

Guidance literature:

In diphenylether; at 220 ℃; for 7h;

DOI:10.1039/c0nj00415d

Reference yield:

5-bromoacenaphthylene-1,2-dione (26254-35-3) → 3-bromo-7,8,9,10-tetraphenylfluoranthene (96765-93-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / methanol

2: diphenylether / 7 h / 220 °C

With potassium hydroxide; In methanol; diphenylether; 2: Diels-Alder reaction;

DOI:10.1039/c0nj00415d

Reference yield:

→ 3-bromo-7,8,9,10-tetraphenylfluoranthene (96765-93-4)

Guidance literature:

3-Brom-7,8,9,10-tetraphenyl-6b,7,10,10a-tetrahydro-7,10-endocarbonyl-fluoranthen, sd. Nitrobenzol;

upstream raw materials:

5-bromoacenaphthylene-1,2-dione

diphenyl acetylene

Downstream raw materials:

N-(naphthalen-1-yl)-N,7,8,9,10-pentaphenylfluoranthen-3-amine

N-(4-tert-butylphenyl)-N-(naphthalen-1-yl)-7,8,9,10-tetraphenylfluoranthen-3-amine

N-phenyl-N-(7,8,9,10-tetraphenylfluoranthen-3-yl)pyren-1-amine

7,8,9,10-tetraphenylfluoranthene-3-carbonitrile