C₃₀H₄₄O₅Si

Base Information

Chemical Name:C₃₀H₄₄O₅Si
CAS No.:1043884-96-3
Molecular Formula:C₃₀H₄₄O₅Si
Molecular Weight:512.762
Hs Code.:

C<sub>30</sub>H<sub>44</sub>O<sub>5</sub>Si

Synonyms:C₃₀H₄₄O₅Si

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Chemical Property of C₃₀H₄₄O₅Si

Chemical Property:

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Technology Process of C₃₀H₄₄O₅Si

There total 5 articles about C₃₀H₄₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85272-31-7
di-tert-butylsilyl bis(trifluoromethanesulfonate)

: 315203-99-7
(2R,3S,5R,6S)-5-(benzyloxy)-6-(2-(benzyloxy)ethyl)-2-(hydroxymethyl)tetrahydro-2H-pyran-3-ol

: 1043884-96-3
C₃₀H₄₄O₅Si

Guidance literature:: With 2,6-dimethylpyridine; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;
DOI:10.1021/ja801576v

Reference yield:

: methyl 3,5-O-di(tert-butyl)silylene-2-deoxy-D-ribofuranoside

: 1043884-96-3
C₃₀H₄₄O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.1: 4-methyl-morpholine / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 21 h / 20 °C

4.1: samarium diiodide / tetrahydrofuran; methanol / 0.5 h / -20 °C / Inert atmosphere

5.1: lithium borohydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

6.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.33 h / 0 °C / Inert atmosphere

6.2: 1 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; lithium borohydride; samarium diiodide; boron trifluoride diethyl etherate; potassium hexamethylsilazane; sodium hydrogencarbonate; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile; 2.1: |Michael Addition;
DOI:10.1021/ol500788c

Reference yield:

: C₁₈H₃₂O₆Si

: 1043884-96-3
C₃₀H₄₄O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: samarium diiodide / tetrahydrofuran; methanol / 0.5 h / -20 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.33 h / 0 °C / Inert atmosphere

3.2: 1 h / 0 °C / Inert atmosphere

With lithium borohydride; samarium diiodide; potassium hexamethylsilazane; In tetrahydrofuran; methanol; toluene;
DOI:10.1021/ol500788c