7-(4-methoxybenzyl)-3-(4-((2-methoxyethoxy) methoxy)benzyl)-3,7-dihydro-2H-diimidazo[4,5-d:4′,5′-f][1,3]diazepin-2-one

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Chemical Name:7-(4-methoxybenzyl)-3-(4-((2-methoxyethoxy) methoxy)benzyl)-3,7-dihydro-2H-diimidazo[4,5-d:4′,5′-f][1,3]diazepin-2-one
CAS No.:1427441-56-2
Molecular Formula:C₂₆H₂₆N₆O₅
Molecular Weight:502.53
Hs Code.:

Synonyms:7-(4-methoxybenzyl)-3-(4-((2-methoxyethoxy) methoxy)benzyl)-3,7-dihydro-2H-diimidazo[4,5-d:4′,5′-f][1,3]diazepin-2-one

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Chemical Property of 7-(4-methoxybenzyl)-3-(4-((2-methoxyethoxy) methoxy)benzyl)-3,7-dihydro-2H-diimidazo[4,5-d:4′,5′-f][1,3]diazepin-2-one

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Technology Process of 7-(4-methoxybenzyl)-3-(4-((2-methoxyethoxy) methoxy)benzyl)-3,7-dihydro-2H-diimidazo[4,5-d:4′,5′-f][1,3]diazepin-2-one

There total 4 articles about 7-(4-methoxybenzyl)-3-(4-((2-methoxyethoxy) methoxy)benzyl)-3,7-dihydro-2H-diimidazo[4,5-d:4′,5′-f][1,3]diazepin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133123-63-4
N-(2-amino-1,2-dicyano-vinyl)-formimydic acid ethyl ester

: 1427441-56-2
7-(4-methoxybenzyl)-3-(4-((2-methoxyethoxy) methoxy)benzyl)-3,7-dihydro-2H-diimidazo[4,5-d:4′,5′-f][1,3]diazepin-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: aniline hydrochloride / ethanol / 3 h / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / ethanol / 3 h / 20 °C

3: acetonitrile / 3 h / 20 °C / Inert atmosphere

4: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C / Inert atmosphere

5: sulfuric acid / acetonitrile / 1 h / Reflux

With sulfuric acid; aniline hydrochloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In ethanol; acetonitrile;
DOI:10.1016/j.bmc.2012.11.050

Reference yield:

: 5-amino-1-(4-methoxybenzyl)-4-cyanoformimidoylimidazole

: 1427441-56-2
7-(4-methoxybenzyl)-3-(4-((2-methoxyethoxy) methoxy)benzyl)-3,7-dihydro-2H-diimidazo[4,5-d:4′,5′-f][1,3]diazepin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 3 h / 20 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C / Inert atmosphere

3: sulfuric acid / acetonitrile / 1 h / Reflux

With sulfuric acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile;
DOI:10.1016/j.bmc.2012.11.050

Reference yield:

: 1427436-23-4
C₁₂H₁₅NO₄

: 1427441-56-2
7-(4-methoxybenzyl)-3-(4-((2-methoxyethoxy) methoxy)benzyl)-3,7-dihydro-2H-diimidazo[4,5-d:4′,5′-f][1,3]diazepin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 3 h / 20 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C / Inert atmosphere

3: sulfuric acid / acetonitrile / 1 h / Reflux

With sulfuric acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile;
DOI:10.1016/j.bmc.2012.11.050