(C₅H₄CH₃)2Mo₂(CO)5(P(C₆H₅)3)

Base Information

• Chemical Name: (C₅H₄CH₃)2Mo₂(CO)5(P(C₆H₅)3)
• CAS No.: 105162-69-4
• Molecular Formula: C₃₅H₂₉Mo₂O₅P
• Molecular Weight: 752.466

Synonyms:(C₅H₄CH₃)2Mo₂(CO)5(P(C₆H₅)3)

Chemical Property of (C₅H₄CH₃)2Mo₂(CO)5(P(C₆H₅)3)

Chemical Property:

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Technology Process of (C₅H₄CH₃)2Mo₂(CO)5(P(C₆H₅)3)

There total 3 articles about (C₅H₄CH₃)2Mo₂(CO)5(P(C₆H₅)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hexacarbonyl-bis(η5-methylcyclopentadienyl)dimolybdenum → (C5H4CH3)2Mo2(CO)5(P(C6H5)3) (105162-69-4)

Guidance literature:

With triphenylphosphine; In cyclohexane; Irradiation (UV/VIS); irrdn. of Mo complex in cyclohexane soln. contg. excess PPh3 at 505, 435, 405, 366 nm;

DOI:10.1021/ja00374a051

Reference yield:

hexacarbonyl-bis(η5-methylcyclopentadienyl)dimolybdenum → (C5H4CH3)2Mo2(CO)5(P(C6H5)3) (105162-69-4) + C5H4CH3Mo(CO)3P(C6H5)3(1+)*C5H4CH3Mo(CO)3(1-)=C5H4CH3Mo(CO)3P(C6H5)3C5H4CH3Mo(CO)3 (105162-71-8)

Guidance literature:

With triphenylphosphine; In dichloromethane; byproducts: CO; Irradiation (UV/VIS); irradiation (λ >525 nm) of a CH2Cl2 soln. of the dimeric Mo complex and PPh3 results in disproportionation and, to a lesser extent, substitution;; not isolated, detected by IR spectroscopy;;

Reference yield:

hexacarbonyl-bis(η5-methylcyclopentadienyl)dimolybdenum → (C5H4CH3)Mo(CO)2(P(C6H5)3)2(1+) (105162-72-9) + (C5H4CH3)2Mo2(CO)5(P(C6H5)3) (105162-69-4) + C5H4CH3Mo(CO)3P(C6H5)3(1+)*C5H4CH3Mo(CO)3(1-)=C5H4CH3Mo(CO)3P(C6H5)3C5H4CH3Mo(CO)3 (105162-71-8)

Guidance literature:

With triphenylphosphine; In benzene; byproducts: CO; Irradiation (UV/VIS); irradiation of a soln. of the Mo complex and PPh3 in benzene or nonpolar solvents ; no reaction at λ > 525 nm, at λ = 290 nm onlythe disubstituted cation is obtained;; not isolated, detected by IR spectroscopy;;

Downstream raw materials:

(C₅H₄CH₃)Mo(CO)2(P(C₆H₅)3)2⁽¹⁺⁾

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