Technology Process of C21H28S2N2O5
There total 4 articles about C21H28S2N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine;
In
dichloromethane;
at 20 ℃;
DOI:10.1002/chem.200601446
- Guidance literature:
-
Multi-step reaction with 14 steps
1: TFA / 0.33 h / 20 °C
2: 1.64 g / benzene / 4 h / Heating
3: 92 percent / BOP-Cl; Et3N / CH2Cl2 / 20 °C
4: TFA / 0.33 h / 20 °C
5: benzene / 4 h / Heating
6: 100 percent / aq. LiOH / tetrahydrofuran / 0.5 h / 20 °C
7: BOP-Cl; Et3N / CH2Cl2 / 20 °C
8: TFA / 0.33 h / 20 °C
9: benzene / 4 h / Heating
10: 99 percent / aq. LiOH / tetrahydrofuran / 0.5 h / 20 °C
11: BOP-Cl; Et3N / CH2Cl2 / 20 °C
12: TFA / 0.33 h / 20 °C
13: benzene / 4 h / Heating
14: 100 percent / tetrahydrofuran; methanol / 20 °C
With
lithium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.1002/chem.200601446
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.64 g / benzene / 4 h / Heating
2: 92 percent / BOP-Cl; Et3N / CH2Cl2 / 20 °C
With
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine;
In
dichloromethane; benzene;
DOI:10.1002/chem.200601446