C₄₄H₆₂O₈Si

Base Information

Chemical Name:C₄₄H₆₂O₈Si
CAS No.:1365268-49-0
Molecular Formula:C₄₄H₆₂O₈Si
Molecular Weight:747.057
Hs Code.:

C<sub>44</sub>H<sub>62</sub>O<sub>8</sub>Si

Synonyms:C₄₄H₆₂O₈Si

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Chemical Property of C₄₄H₆₂O₈Si

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Technology Process of C₄₄H₆₂O₈Si

There total 10 articles about C₄₄H₆₂O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1365268-48-9
C₄₂H₅₈O₇Si

: 107-30-2
chloromethyl methyl ether

: 1365268-49-0
C₄₄H₆₂O₈Si

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; at 50 ℃;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: C₁₉H₂₄O₂

: 1365268-49-0
C₄₄H₆₂O₈Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene-4-sulfonic acid / benzene / Reflux

2.1: n-butyllithium / tetrahydrofuran / -78 °C

2.2: -78 - 20 °C

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 20 °C

3.2: 0 °C

3.3: -78 °C

4.1: 1H-imidazole / dichloromethane / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 60 °C

6.1: diisobutylaluminium hydride / dichloromethane / -78 °C

7.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

8.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

9.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

9.2: -78 °C

10.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

With 1H-imidazole; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; water; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; 1,2-dichloro-ethane; benzene;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: 1365268-46-7
C₄₀H₅₄O₅Si

: 1365268-49-0
C₄₄H₆₂O₈Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

3.2: -78 °C

4.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2012.01.058