(2R),(3S)-4-(tert-butyldimethylsilyloxy)-2,3-dihydroxy-2,3-O-isopropylidene-1-butanethiol

Base Information

Chemical Name:(2R),(3S)-4-(tert-butyldimethylsilyloxy)-2,3-dihydroxy-2,3-O-isopropylidene-1-butanethiol
CAS No.:191671-45-1
Molecular Formula:C₁₃H₂₈O₃SSi
Molecular Weight:292.515
Hs Code.:

Synonyms:(2R),(3S)-4-(tert-butyldimethylsilyloxy)-2,3-dihydroxy-2,3-O-isopropylidene-1-butanethiol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R),(3S)-4-(tert-butyldimethylsilyloxy)-2,3-dihydroxy-2,3-O-isopropylidene-1-butanethiol

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Technology Process of (2R),(3S)-4-(tert-butyldimethylsilyloxy)-2,3-dihydroxy-2,3-O-isopropylidene-1-butanethiol

There total 1 articles about (2R),(3S)-4-(tert-butyldimethylsilyloxy)-2,3-dihydroxy-2,3-O-isopropylidene-1-butanethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51490-01-8
1-(3,4,5-trimethoxyphenyl)-2-bromoethanone

: 191671-42-8
3',4',5'-Trimethoxy-2-[(2R),(3S)-2,3,4-trihydroxy-butylthio]acetophenone

: 191671-45-1
(2R),(3S)-4-(tert-butyldimethylsilyloxy)-2,3-dihydroxy-2,3-O-isopropylidene-1-butanethiol

Guidance literature:

Reference yield:

: 191671-45-1
(2R),(3S)-4-(tert-butyldimethylsilyloxy)-2,3-dihydroxy-2,3-O-isopropylidene-1-butanethiol

: Toluene-4-sulfonic acid (4R,5S)-5-[(3aS,4S,6R,6aR)-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethylsulfanylmethyl]-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide

2: Bu₄NF / tetrahydrofuran

3: pyridine

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja9905391