(4-hydroxymethyl-benzyl)-carbamic acid-(2-hydroxy-ethyl ester)

Base Information

• Chemical Name: (4-hydroxymethyl-benzyl)-carbamic acid-(2-hydroxy-ethyl ester)
• CAS No.: 103565-62-4
• Molecular Formula: C₁₁H₁₅NO₄
• Molecular Weight: 225.244
• Mol file: 103565-62-4.mol

Synonyms:(4-hydroxymethyl-benzyl)-carbamic acid-(2-hydroxy-ethyl ester)

Chemical Property of (4-hydroxymethyl-benzyl)-carbamic acid-(2-hydroxy-ethyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4-hydroxymethyl-benzyl)-carbamic acid-(2-hydroxy-ethyl ester)

There total 3 articles about (4-hydroxymethyl-benzyl)-carbamic acid-(2-hydroxy-ethyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-hydroxymethyl-benzylamine (39895-56-2) → (4-hydroxymethyl-benzyl)-carbamic acid-(2-hydroxy-ethyl ester) (103565-62-4)

Guidance literature:

DOI:10.1021/ja01560a045

Reference yield:

methyl-4-carbamoylbenzoate (6757-31-9) → (4-hydroxymethyl-benzyl)-carbamic acid-(2-hydroxy-ethyl ester) (103565-62-4)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄

With lithium aluminium tetrahydride;

DOI:10.1021/ja01560a045

Reference yield:

Monomethyl terephthalate (1679-64-7) → (4-hydroxymethyl-benzyl)-carbamic acid-(2-hydroxy-ethyl ester) (103565-62-4)

Guidance literature:

Multi-step reaction with 3 steps

1: SOCl₂ / anschliessendes Behandeln mit NH₃

2: LiAlH₄

With lithium aluminium tetrahydride; thionyl chloride;

DOI:10.1021/ja01560a045

upstream raw materials:

4-hydroxymethyl-benzylamine

methyl-4-carbamoylbenzoate

Monomethyl terephthalate