o-amino-N-2-propenylbenzenesulfonamide

Base Information

• Chemical Name: o-amino-N-2-propenylbenzenesulfonamide
• CAS No.: 107616-16-0
• Molecular Formula: C₉H₁₂N₂O₂S
• Molecular Weight: 212.272
• Mol file: 107616-16-0.mol

Synonyms:o-amino-N-2-propenylbenzenesulfonamide

Chemical Property of o-amino-N-2-propenylbenzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of o-amino-N-2-propenylbenzenesulfonamide

There total 2 articles about o-amino-N-2-propenylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N-allyl-o-nitrobenzenesulfonamide (65118-17-4) → o-amino-N-2-propenylbenzenesulfonamide (107616-16-0)

Guidance literature:

With hydrogenchloride; water; iron; In benzene; for 3h; Heating;

DOI:10.1021/jo00386a007

Reference yield:

2-Nitrobenzenesulfonyl chloride (1694-92-4) → o-amino-N-2-propenylbenzenesulfonamide (107616-16-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / K₂CO₃ / CH₂Cl₂ / 2 h

2: 80 percent / Fe, conc. HCl, H₂O / benzene / 3 h / Heating

With hydrogenchloride; water; iron; potassium carbonate; In dichloromethane; benzene;

DOI:10.1021/jo00386a007

Reference yield: 58.0%

o-amino-N-2-propenylbenzenesulfonamide (107616-16-0) → o-(N-2-propenylsulfamoyl)benzenediazonium tetrafluoroborate

Guidance literature:

With tetrafluoroboric acid; sodium nitrite; In water;

DOI:10.1021/jo00386a007

upstream raw materials:

N-allyl-o-nitrobenzenesulfonamide

2-Nitrobenzenesulfonyl chloride