C₆₀H₉₆NO₁₁PSi

Base Information

Chemical Name:C₆₀H₉₆NO₁₁PSi
CAS No.:865302-38-1
Molecular Formula:C₆₀H₉₆NO₁₁PSi
Molecular Weight:1066.48
Hs Code.:

C<sub>60</sub>H<sub>96</sub>NO<sub>11</sub>PSi

Synonyms:C₆₀H₉₆NO₁₁PSi

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Chemical Property of C₆₀H₉₆NO₁₁PSi

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Technology Process of C₆₀H₉₆NO₁₁PSi

There total 23 articles about C₆₀H₉₆NO₁₁PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 865302-36-9
(2R,3R)-3-Z-[(4R,5R)-5-(2Z-octenyl)-2-oxo-4-[(1,1-dimethylethyl)diphenylsilyloxy]cyclopentylidenemethyl]oxirane-2-butanoic acid

: 17364-16-8,17364-17-9,17364-18-0,14863-27-5
1-palmitoyl-sn-glycero-3-phosphocholine

: 865302-38-1
C₆₀H₉₆NO₁₁PSi

Guidance literature:: With dmap; 2,4,6-trichlorobenzoyl chloride; In chloroform; at -40 - 22 ℃; for 1h;
DOI:10.1021/ol051415y

Reference yield:

: 111-29-5
1 ,5-pentanediol

: 865302-38-1
C₆₀H₉₆NO₁₁PSi

Guidance literature:: Multi-step reaction with 12 steps

1.1: 94 percent / TMSOTf / acetonitrile / 0.5 h / -23 °C

2.1: 100 percent / oxalyl chloride; DMSO; triethylamine / CH₂Cl₂ / -78 - 22 °C

3.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

3.2: 91 percent / tetrahydrofuran / 0.33 h / 22 °C

4.1: 100 percent / diisobutylaluminum hydride / cyclohexane; CH₂Cl₂ / 0.33 h / -78 °C

5.1: 94 percent / titanium tetraisopropoxide; tert-butyl hydroperoxide; molecular sieves 4 Angstroem / D-(-)-diisopropyl tartrate / CH₂Cl₂; decane / -20 - 0 °C

6.1: pyridine; Dess-Martin periodinane / benzene; acetonitrile / 0.67 h / 22 °C

7.1: tert-butyllithium / pentane; diethyl ether / 1 h / -78 °C

7.2: 75 percent / pentane; diethyl ether / 0.75 h / -78 °C

8.1: formic acid / tetrahydrofuran; H₂O / 0.75 h / 22 °C

9.1: 89 percent / DDQ / CH₂Cl₂ / 1 h / 22 °C / pH 7

10.1: pyridine; Dess-Martin periodinane / benzene; acetonitrile / 0.67 h / 22 °C

11.1: 100 percent / 2-methyl-2-butene; sodium chlorite; sodium dihydrogen phosphate / 2-methyl-propan-2-ol; H₂O / 1 h / 22 °C

12.1: 88 percent / DMAP; 2,4,6-trichlorobenzoyl chloride / CHCl₃ / 1 h / -40 - 22 °C

With pyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; sodium chlorite; formic acid; sodium dihydrogen phosphate; 2-methyl-but-2-ene; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; 2,4,6-trichlorobenzoyl chloride; tert.-butyl lithium; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; D-(-)-diisopropyl tartrate; In tetrahydrofuran; diethyl ether; decane; dichloromethane; chloroform; cyclohexane; water; acetonitrile; tert-butyl alcohol; pentane; benzene; 2.1: Swern oxidation / 3.2: Horner-Emmons reaction / 5.1: Sharpless asymmetric epoxidation;
DOI:10.1021/ol051415y

Reference yield:

: 131375-63-8
5-(4-methoxybenzyloxy)-1-pentanol

: 865302-38-1
C₆₀H₉₆NO₁₁PSi

Guidance literature:: Multi-step reaction with 11 steps

1.1: 100 percent / oxalyl chloride; DMSO; triethylamine / CH₂Cl₂ / -78 - 22 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

2.2: 91 percent / tetrahydrofuran / 0.33 h / 22 °C

3.1: 100 percent / diisobutylaluminum hydride / cyclohexane; CH₂Cl₂ / 0.33 h / -78 °C

4.1: 94 percent / titanium tetraisopropoxide; tert-butyl hydroperoxide; molecular sieves 4 Angstroem / D-(-)-diisopropyl tartrate / CH₂Cl₂; decane / -20 - 0 °C

5.1: pyridine; Dess-Martin periodinane / benzene; acetonitrile / 0.67 h / 22 °C

6.1: tert-butyllithium / pentane; diethyl ether / 1 h / -78 °C

6.2: 75 percent / pentane; diethyl ether / 0.75 h / -78 °C

7.1: formic acid / tetrahydrofuran; H₂O / 0.75 h / 22 °C

8.1: 89 percent / DDQ / CH₂Cl₂ / 1 h / 22 °C / pH 7

9.1: pyridine; Dess-Martin periodinane / benzene; acetonitrile / 0.67 h / 22 °C

10.1: 100 percent / 2-methyl-2-butene; sodium chlorite; sodium dihydrogen phosphate / 2-methyl-propan-2-ol; H₂O / 1 h / 22 °C

11.1: 88 percent / DMAP; 2,4,6-trichlorobenzoyl chloride / CHCl₃ / 1 h / -40 - 22 °C

With pyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; sodium chlorite; formic acid; sodium dihydrogen phosphate; 2-methyl-but-2-ene; oxalyl dichloride; 4 A molecular sieve; 2,4,6-trichlorobenzoyl chloride; tert.-butyl lithium; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; D-(-)-diisopropyl tartrate; In tetrahydrofuran; diethyl ether; decane; dichloromethane; chloroform; cyclohexane; water; acetonitrile; tert-butyl alcohol; pentane; benzene; 1.1: Swern oxidation / 2.2: Horner-Emmons reaction / 4.1: Sharpless asymmetric epoxidation;
DOI:10.1021/ol051415y