2,3,4-tri-O-acetyl-6-O-2-nitrobenzyl-α-D-galactopyranosyl hydrogenphosphonate triethylammonium salt

Base Information

• Chemical Name: 2,3,4-tri-O-acetyl-6-O-2-nitrobenzyl-α-D-galactopyranosyl hydrogenphosphonate triethylammonium salt
• CAS No.: 1023293-30-2
• Molecular Formula: C₆H₁₅N*C₁₉H₂₄NO₁₃P
• Molecular Weight: 606.564

Synonyms:2,3,4-tri-O-acetyl-6-O-2-nitrobenzyl-α-D-galactopyranosyl hydrogenphosphonate triethylammonium salt

Chemical Property of 2,3,4-tri-O-acetyl-6-O-2-nitrobenzyl-α-D-galactopyranosyl hydrogenphosphonate triethylammonium salt

Chemical Property:

Purity/Quality:

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Technology Process of 2,3,4-tri-O-acetyl-6-O-2-nitrobenzyl-α-D-galactopyranosyl hydrogenphosphonate triethylammonium salt

There total 1 articles about 2,3,4-tri-O-acetyl-6-O-2-nitrobenzyl-α-D-galactopyranosyl hydrogenphosphonate triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

2,3,4-tri-O-acetyl-6-O-2-nitrobenzyl-D-galactopyranose + triethylamine (121-44-8) → 2,3,4-tri-O-acetyl-6-O-2-nitrobenzyl-α-D-galactopyranosyl hydrogenphosphonate triethylammonium salt (1023293-30-2)

Guidance literature:

With 1H-imidazole; phosphorus trichloride; In acetonitrile; at 0 - 20 ℃; for 0.75h;

DOI:10.1016/j.carres.2008.01.021

Reference yield:

2,3,4-tri-O-acetyl-6-O-2-nitrobenzyl-α-D-galactopyranosyl hydrogenphosphonate triethylammonium salt (1023293-30-2) + 9-Fluorenylmethanol (24324-17-2) → C6H15N*C33H34NO14P

Guidance literature:

2,3,4-tri-O-acetyl-6-O-2-nitrobenzyl-α-D-galactopyranosyl hydrogenphosphonate triethylammonium salt; 9-Fluorenylmethanol; With pyridine; pivaloyl chloride; at 20 ℃; for 3h;

With pyridine; iodine; In water; at -40 - 0 ℃; Further stages.;

DOI:10.1016/j.carres.2008.01.021

upstream raw materials:

triethylamine

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