Technology Process of C21H25NO6
There total 2 articles about C21H25NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C20H25NO7;
With
potassium carbonate;
In
methanol;
at 20 ℃;
for 0.166667h;
dimethyl 1-(1-diazo-2-oxopropyl)phosphonate;
In
methanol;
at 20 ℃;
for 2h;
DOI:10.1021/ja2104679
- Guidance literature:
-
Multi-step reaction with 2 steps
2.1: potassium carbonate / methanol / 0.17 h / 20 °C
2.2: 2 h / 20 °C
With
potassium carbonate;
In
methanol;
1.1: Swern oxidation;
DOI:10.1021/ja2104679
- Guidance literature:
-
Multi-step reaction with 6 steps
1: copper(II) sulfate; sodium L-ascorbate / methanol; water
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 0 - 4 °C
3: lithium perchlorate / acetonitrile / 20 h / 70 °C
4: triethylamine / dichloromethane / 20 h
5: palladium 10% on activated carbon; hydrogen / methanol / 5 h
6: triethylamine / dichloromethane / 20 h
With
palladium 10% on activated carbon; hydrogen; lithium perchlorate; copper(II) sulfate; sodium L-ascorbate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ja2104679