(E)-1-(4-Benzyloxy-2-hydroxy-phenyl)-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-propenone

Base Information

• Chemical Name: (E)-1-(4-Benzyloxy-2-hydroxy-phenyl)-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-propenone
• CAS No.: 96755-09-8
• Molecular Formula: C₂₄H₂₀O₅
• Molecular Weight: 388.42

Synonyms:(E)-1-(4-Benzyloxy-2-hydroxy-phenyl)-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-propenone

Chemical Property of (E)-1-(4-Benzyloxy-2-hydroxy-phenyl)-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-propenone

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Technology Process of (E)-1-(4-Benzyloxy-2-hydroxy-phenyl)-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-propenone

There total 1 articles about (E)-1-(4-Benzyloxy-2-hydroxy-phenyl)-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

1-[4-(benzyloxy)-2-hydroxyphenyl]ethanone (29682-12-0) + 2,3-dihydro-benzo[1,4]dioxin-6-carbaldehyde (29668-44-8) → (E)-1-(4-Benzyloxy-2-hydroxy-phenyl)-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-propenone (96755-09-8)

Guidance literature:

With potassium hydroxide; In ethanol; Ambient temperature;

Reference yield: 80.0%

(E)-1-(4-Benzyloxy-2-hydroxy-phenyl)-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-propenone (96755-09-8) → 7-Benzyloxy-2-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-chromen-4-one (96754-57-3)

Guidance literature:

With selenium(IV) oxide; In pentan-1-ol; Heating;

Reference yield: 40.0%

(E)-1-(4-Benzyloxy-2-hydroxy-phenyl)-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-propenone (96755-09-8) → 2-(2,3-dihydro-benzo[1,4]dioxan-6-yl)-3-hydroxy-7-benzyloxy-benzopyran-4-one (96754-61-9) + 7-Benzyloxy-2-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-3-hydroxy-chroman-4-one (96754-64-2)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; In methanol; for 48h; Ambient temperature;

upstream raw materials:

1-[4-(benzyloxy)-2-hydroxyphenyl]ethanone

2,3-dihydro-benzo[1,4]dioxin-6-carbaldehyde

Downstream raw materials:

7-Benzyloxy-3-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-chromen-4-one

7-Benzyloxy-2-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-chromen-4-one

2-(2,3-dihydro-benzo[1,4]dioxan-6-yl)-3-hydroxy-7-benzyloxy-benzopyran-4-one

7-Benzyloxy-2-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-3-hydroxy-chroman-4-one

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