Technology Process of C27H30F2N4O4
There total 6 articles about C27H30F2N4O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
ethanol; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium periodate / rhodium(III) chloride hydrate / ethyl acetate; acetonitrile; water / 18 h / 20 °C
2: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 0 - 20 °C
3: water; lithium hydroxide monohydrate / methanol
4: hydrogenchloride / ethanol; water
With
hydrogenchloride; sodium periodate; lithium hydroxide monohydrate; water; benzotriazol-1-ol; dicyclohexyl-carbodiimide;
rhodium(III) chloride hydrate;
In
methanol; ethanol; dichloromethane; water; ethyl acetate; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / dmap / tetrahydrofuran / 0 - 20 °C
2: sodium periodate / rhodium(III) chloride hydrate / ethyl acetate; acetonitrile; water / 18 h / 20 °C
3: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 0 - 20 °C
4: water; lithium hydroxide monohydrate / methanol
5: hydrogenchloride / ethanol; water
With
pyridine; hydrogenchloride; sodium periodate; lithium hydroxide monohydrate; water; benzotriazol-1-ol; dicyclohexyl-carbodiimide;
dmap; rhodium(III) chloride hydrate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; acetonitrile;